Sonochemical synthesis of Prussian blue nanocubes from a single-source precursor

被引：150
|
作者：
Wu, XL
Cao, MH [1 ]
Hu, CW
He, XY
机构：
[1] NE Normal Univ, Dept Chem, Changchun 130024, Peoples R China
[2] Beijing Inst Technol, Inst Chem Phys, Beijing 100081, Peoples R China
[3] Beijing Inst Technol, Dept Chem, Beijing 100081, Peoples R China
来源：
CRYSTAL GROWTH & DESIGN | 2006年 / 6卷 / 01期
关键词：
D O I：
10.1021/cg050371x
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Regular, single-crystalline nanocubes of Prussian blue, Fe-4[Fe(CN)(6)](3), with different sizes were synthesized in large quantities by a direct dissociation of the single-source precursor K4Fe(CN)(6) in acidic solution under ultrasonic conditions. The size and size distribution of the cubes strongly depends on the reaction temperature, the concentration of K4Fe(CN)(6) aqueous solution, and the ultrasonic condition. The probable mechanism of formation of Prussian blue is discussed.
引用
收藏
页码：26 / 28
页数：3
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