Comparison of extraction techniques for gas chromatographic determination of volatile carhonyl compounds in alcohols

被引：19
|
作者：
Wardencki, W [1 ]
Orlita, J [1 ]
Namiesnik, J [1 ]
机构：
[1] Gdansk Univ Technol, Fac Chem, Dept Analyt Chem, PL-80952 Gdansk, Poland
来源：
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 2001年 / 369卷 / 7-8期
关键词：
D O I：
10.1007/s002160100738
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Two extraction procedures, i.e. conventional liquid-liquid extraction (LLE) and liquid solid-phase microextraction (SPME) for extraction of the oximes formed after derivatization of carbonyl compounds with omicron-(2,3, 4,5,6-pentafluorobenzyl) hydroxylamine (PFBHA) in alcoholic solutions have been compared. The limit of detection for LLE followed by GC-ECD determination of C-1-C-6 was in the range of 0.23-3.3 mug/L, whereas for liquid SPME 0.005-0.33 mug/L. Both methods elaborated can be applied to the determination of carbonyl compounds present in spirits and alcoholic beverages.
引用
下载
收藏
页码：661 / 665
页数：5
相关论文
共 50 条
  • [41] GAS-CHROMATOGRAPHIC DETERMINATION OF METHANAL TRACES IN PRESENCE OF OTHER VOLATILE CARBONYL-COMPOUNDS
    MERAT, E
    JOURNAL OF CHROMATOGRAPHY, 1978, 153 (02): : 530 - 531
  • [42] GAS CHROMATOGRAPHIC-MASS SPECTROMETRIC DETERMINATION OF VOLATILE ORGANIC-COMPOUNDS IN AN URBAN ATMOSPHERE
    IOFFE, BV
    ISIDOROV, VA
    ZENKEVICH, IG
    JOURNAL OF CHROMATOGRAPHY, 1977, 142 (NOV): : 787 - 795
  • [43] Comparison of different extraction techniques for the determination of polychlorinated organic compounds in sediment
    D. Martens
    M. Gfrerer
    T. Wenzl
    A. Zhang
    B. Gawlik
    K.-W. Schramm
    E. Lankmayr
    A. Kettrup
    Analytical and Bioanalytical Chemistry, 2002, 372 : 562 - 568
  • [44] Comparison of different extraction techniques for the determination of polychlorinated organic compounds in sediment
    Martens, D
    Gfrerer, M
    Wenzl, T
    Zhang, A
    Gawlik, BM
    Schramm, KW
    Lankmayr, E
    Kettrup, A
    ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2002, 372 (04) : 562 - 568
  • [45] GAS-CHROMATOGRAPHIC DETERMINATION OF VOLATILE NITROSAMINES IN FOODS
    ESSIGMAN.JM
    ISSENBER.P
    JOURNAL OF FOOD SCIENCE, 1972, 37 (05) : 684 - &
  • [46] GAS-CHROMATOGRAPHIC DETERMINATION OF SOLUBILITY IN VOLATILE LIQUIDS
    KURKCHI, GA
    IOGANSEN, AV
    RUSSIAN JOURNAL OF PHYSICAL CHEMISTRY,USSR, 1966, 40 (11): : 1575 - &
  • [47] EXTRACTION-GAS CHROMATOGRAPHIC METHOD FOR THE DETERMINATION OF ORGANOPHOSPHORUS COMPOUNDS AS LUBRICATING OIL ADDITIVES
    HABBOUSH, AE
    FARROHA, SM
    KHALAF, HI
    JOURNAL OF CHROMATOGRAPHY A, 1995, 696 (02) : 257 - 263
  • [48] Gas-Chromatographic Determination of Organic Compounds in Water with the Use of Supercritical Fluid Extraction
    I. N. Glazkov
    I. A Revel'skii
    S. V. Kuzyakin
    Yu. A. Zolotov
    Journal of Analytical Chemistry, 2004, 59 : 1085 - 1090
  • [49] Gas-chromatographic determination of organic compounds in water with the use of supercritical fluid extraction
    Glazkov, IN
    Revel'skii, IA
    Kuzyakin, SV
    Zolotov, YA
    JOURNAL OF ANALYTICAL CHEMISTRY, 2004, 59 (11) : 1085 - 1090
  • [50] Determination of volatile organic compounds in river water by solid phase extraction and gas chromatography
    M.A.Mottaleb
    M.Z.Abedin
    M.S.Islam
    Journal of Environmental Sciences, 2004, (03) : 497 - 501
12345