Comparison of different extraction techniques for the determination of polychlorinated organic compounds in sediment

被引：57

作者：

Martens, D ^{[1
]}

Gfrerer, M

Wenzl, T

Zhang, A

Gawlik, BM

Schramm, KW

Lankmayr, E

Kettrup, A

机构：

[1] Tech Univ Munich, Dept Ecol Chem & Environm Analyt Chem, D-85350 Freising Weihenstephan, Germany

[2] Graz Univ Technol, Inst Analyt Chem Micro & Radiochem, A-8010 Graz, Austria

[3] Nanjing Univ, Sch Environm, Nanjing 210008, Peoples R China

[4] Commiss European Communities, DG Joint Res Ctr, Inst Reference Mat & Measurements, B-2440 Geel, Belgium

[5] GSF, Natl Ctr Environm & Hlth, Inst Ecol Chem, D-85764 Neuherberg, Germany

来源：

ANALYTICAL AND BIOANALYTICAL CHEMISTRY | 2002年 / 372卷 / 04期

关键词：

soxhlet extraction; ASE; microwave-assisted extraction; ultrasonic extraction; fluidized-bed extraction; chlorinated compounds;

D O I：

10.1007/s00216-001-1120-y

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The performance of various enhanced extraction techniques, such as accelerated solvent extraction, microwave-assisted extraction, Soxhlet extraction, ultrasonic extraction and fluidized-bed extraction for the determination of polychlorinated organic compounds in dry sediment was investigated in two laboratories. The results of the two laboratories were in good agreement. The extraction yields from the batch extraction methods were lower than those from the dynamic techniques. Accelerated solvent extraction, especially, exhibited higher extraction efficiency than the standard procedure, Soxhlet extraction, whereas the results of fluidized-bed extraction were comparable.

引用

页码：562 / 568

页数：7

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