Use of solid-phase microextraction for the detection of acetic acid by ion-trap gas chromatography-mass spectrometry and application to indoor levels in museums

被引：23
|
作者：
Godoi, AFL [1 ]
Van Vaeck, L [1 ]
Van Grieken, R [1 ]
机构：
[1] Univ Antwerp, Micro & Trace Anal Ctr, Dept Chem, CDE, B-2610 Antwerp, Belgium
来源：
JOURNAL OF CHROMATOGRAPHY A | 2005年 / 1067卷 / 1-2期
关键词：
SPME; acetic acid; museum; GC-MS;
D O I：
10.1016/j.chroma.2004.12.054
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A simple and efficient method using solid-phase microextraction (SPME) and gas chromatography-ion trap mass spectrometry (GC-ITMS) was developed for the analysis of acetic acid in air. The choice of the SPME fibre revealed to be critical as well as the sampling and desorption time. A dilution vessel was used for calibration. The precision of the method was found to be 4.7% relative standard deviation (RSD) and the detection limit 5.7 mu g m(-3). The SPME-GC-MS technique was applied to the analysis of acetic acid in museum atmospheres. (c) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码：331 / 336
页数：6
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