Synthesis and Properties of C,N-Chelated Carbene Complexes of Palladium(II) with 2-Aminobenzo[d]thiazole Fragment
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作者:
Mikherdov, A. S.
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St Petersburg State Univ, Univ Skaya Nab 7-9, St Petersburg 199034, RussiaSt Petersburg State Univ, Univ Skaya Nab 7-9, St Petersburg 199034, Russia
Mikherdov, A. S.
[1
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Baikov, S. V.
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St Petersburg State Univ, Univ Skaya Nab 7-9, St Petersburg 199034, RussiaSt Petersburg State Univ, Univ Skaya Nab 7-9, St Petersburg 199034, Russia
Baikov, S. V.
[1
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Proskurina, I. K.
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KD Ushinskii Yaroslavl State Pedag Univ, M Dorogov Ctr Transfer Pharmaceut Technol, Yaroslavl, RussiaSt Petersburg State Univ, Univ Skaya Nab 7-9, St Petersburg 199034, Russia
Proskurina, I. K.
[2
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Shetnev, A. A.
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KD Ushinskii Yaroslavl State Pedag Univ, M Dorogov Ctr Transfer Pharmaceut Technol, Yaroslavl, RussiaSt Petersburg State Univ, Univ Skaya Nab 7-9, St Petersburg 199034, Russia
Shetnev, A. A.
[2
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Kotov, A. D.
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KD Ushinskii Yaroslavl State Pedag Univ, M Dorogov Ctr Transfer Pharmaceut Technol, Yaroslavl, RussiaSt Petersburg State Univ, Univ Skaya Nab 7-9, St Petersburg 199034, Russia
Kotov, A. D.
[2
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机构:
[1] St Petersburg State Univ, Univ Skaya Nab 7-9, St Petersburg 199034, Russia
[2] KD Ushinskii Yaroslavl State Pedag Univ, M Dorogov Ctr Transfer Pharmaceut Technol, Yaroslavl, Russia
The reaction of bis(cyclohexylisocyanide) complex of Pd(II) with substituted benzo[d]thiazole-2-amines in the presence of triethanolamine as the base has lead to the formation of deprotonated C,N-chelated carbene complexes with a structure similar to that described previously for the products of the reaction with unsubstituted benzo[d]thiazole-2-amine. The complexes have been isolated and characterized using high-resolution mass spectrometry, IR and NMR spectroscopy (H-1, C-13{H-1}, H-1-H-1 COSY, H-1-H-1 NOESY, H-1-C-13 HSQC, H-1-C-13 HMBC). The resulting complexes have exhibited moderate antibacterial activity against sensitive strains of gram-negative bacteria E. coli (C600) and P. fluorescens (P218), gram-positive bacteria S. aureus (ATCC-25923) and B. subtillis (B-3142D) as well as fungi C. albicans (401/NCTC-885-653).
机构:
Univ Louis Pasteur Strasbourg 1, CNRS, UMR 7177, Lab DECOMET,Inst Le Bel, F-67000 Strasbourg, FranceUniv Louis Pasteur Strasbourg 1, CNRS, UMR 7177, Lab DECOMET,Inst Le Bel, F-67000 Strasbourg, France
Fliedel, Christophe
Maisse-Francois, Aline
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Univ Louis Pasteur Strasbourg 1, CNRS, UMR 7177, Lab DECOMET,Inst Le Bel, F-67000 Strasbourg, FranceUniv Louis Pasteur Strasbourg 1, CNRS, UMR 7177, Lab DECOMET,Inst Le Bel, F-67000 Strasbourg, France
Maisse-Francois, Aline
Bellemin-Laponnaz, Stephane
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Univ Louis Pasteur Strasbourg 1, CNRS, UMR 7177, Lab DECOMET,Inst Le Bel, F-67000 Strasbourg, FranceUniv Louis Pasteur Strasbourg 1, CNRS, UMR 7177, Lab DECOMET,Inst Le Bel, F-67000 Strasbourg, France