(E)-5-(2-Chlorophenyl)-7-ethyl-2-oxo-2,3-dihydro-1H-thieno[2,3-e][1,4]diazepin-4-ium 2,4,6-trinitrophenolate

被引：1

作者：

Betz, Richard ^{[1
]}

Gerber, Thomas ^{[1
]}

Hosten, Eric ^{[1
]}

Dayananda, Alaloor S. ^{[2
]}

Yathirajan, Hemmige S. ^{[2
]}

Ramesha, A. R. ^{[3
]}

机构：

[1] Nelson Mandela Metropolitan Univ, Dept Chem, Port Elizabeth, South Africa

[2] Univ Mysore, Dept Studies Chem, Mysore 570006, Karnataka, India

[3] RL Fine Chem, Bangalore 560064, Karnataka, India

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2012年 / 68卷

关键词：

GRAPH-SET ANALYSIS; CRYSTALS; PATTERNS;

D O I：

10.1107/S1600536812002607

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title molecular salt, C15H14ClN2OS+center dot C6H2N3O7-, protonation occurred on the double-bonded N atom. One of the nitro groups shows slight disorder over two orientations, with an occupancy ratio of 0.91:0.09. In the crystal, classical N-H center dot center dot center dot O hydrogen bonds, as well as C-H center dot center dot center dot O contacts connect the components into a three-dimensional network. The seven-membered ring adopts a boat-like conformation. The least-squares plane defined by its non-H atoms encloses an angle of 38.99 (6)degrees with the benzene ring bonded to it.

引用

页码：O516 / U1668

页数：13

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