(E)-5-(2-Chlorophenyl)-7-ethyl-2-oxo-2,3-dihydro-1H-thieno[2,3-e][1,4]diazepin-4-ium 2,4,6-trinitrophenolate

被引：1

作者：

Betz, Richard ^{[1
]}

Gerber, Thomas ^{[1
]}

Hosten, Eric ^{[1
]}

Dayananda, Alaloor S. ^{[2
]}

Yathirajan, Hemmige S. ^{[2
]}

Ramesha, A. R. ^{[3
]}

机构：

[1] Nelson Mandela Metropolitan Univ, Dept Chem, Port Elizabeth, South Africa

[2] Univ Mysore, Dept Studies Chem, Mysore 570006, Karnataka, India

[3] RL Fine Chem, Bangalore 560064, Karnataka, India

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2012年 / 68卷

关键词：

GRAPH-SET ANALYSIS; CRYSTALS; PATTERNS;

D O I：

10.1107/S1600536812002607

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title molecular salt, C15H14ClN2OS+center dot C6H2N3O7-, protonation occurred on the double-bonded N atom. One of the nitro groups shows slight disorder over two orientations, with an occupancy ratio of 0.91:0.09. In the crystal, classical N-H center dot center dot center dot O hydrogen bonds, as well as C-H center dot center dot center dot O contacts connect the components into a three-dimensional network. The seven-membered ring adopts a boat-like conformation. The least-squares plane defined by its non-H atoms encloses an angle of 38.99 (6)degrees with the benzene ring bonded to it.

引用

页码：O516 / U1668

页数：13

共 50 条

[21] New Cyclopenta[4′,5′] pyrido[3′,2′:4,5]thieno[2,3-e][1,2,4]triazolo[4,3-c]pyrimidines and Cyclopenta[4′,5′]pyrido[3′,2′:4,5]thieno[2,3-e][1,2,4]triazolo[1,5-c]pyrimidines: Synthesis and Antimicrobial Activities
Sirakanyan, Samvel N.
Spinelli, Domenico
Geronikaki, Athina
Kartsev, Viktor G.
Hakobyan, Elmira K.
Panosyan, Henrik A.
Stepanyan, Hrachya M.
Zuppiroli, Luca
Hovakimyan, Anush A.
CURRENT ORGANIC CHEMISTRY, 2017, 21 (13) : 1227 - 1241
[22] 1,4-Diazoniabicyclo[2.2.2]octane bis(2,4,6-trinitrophenolate)
SiMa, Weiwei
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1584 - U685
[23] SYNTHESIS AND BIOLOGICAL-ACTIVITY OF PYRIDO[2,3-E]-1,4 DIAZEPINE AND PYRIDO[2,3-B][1,4]DIAZEPINE
CARBONI, S
DASETTIMO, A
BERTINI, D
FERRARINI, PL
LIVI, O
TONETTI, I
FARMACO-EDIZIONE SCIENTIFICA, 1975, 30 (04): : 237 - 247
[24] SYNTHESIS OF 3-ALKYL-5-PHENYL-2-THIOXO-3H-1,2-DIHYDRO-CYCLOALKA[4,5]THIENO[2,3-E][1,2,4]TRIAZEPINES
RICHTER, P
OERTEL, D
OERTEL, F
PHARMAZIE, 1988, 43 (11): : 753 - 755
[25] Short Synthesis of Enantiopure Thieno[2,3-f]triazolo[1,5-a][1,4]diazepines and Thieno[2,3-f][1,4]diazepin-5-ones
Molteni, Giorgio
JOURNAL OF HETEROCYCLIC CHEMISTRY, 2014, 51 : E329 - E331
[26] 2-(2-Chlorophenyl)-2,3-dihydroquinazolin-4(1H)-one
Li, Ming-Jian
Feng, Chang-Jun
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O2145 - U1949
[27] SYNTHESIS AND REACTIVITY OF FURO[2,3-E]PYRROLO[1,2-A][1,4]DIAZEPIN-9-ONE
POVAZANEC, F
DECROIX, B
MOREL, J
JOURNAL OF HETEROCYCLIC CHEMISTRY, 1992, 29 (06) : 1507 - 1512
[28] 3-(2-Chloroethyl)-2-methyl-4-oxo-4H-pyrido[1,2-a]pyrimidinium 2,4,6-trinitrophenolate
Jasinski, Jerry P.
Butcher, Ray J.
Al-Arique, Q. N. M. Hakim
Yathirajan, H. S.
Narayana, B.
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O2201 - U2434
[29] N-(4-Chlorophenyl)-5-(4,5-dihydro-1H-imidazol-2-yl)thieno[2,3-b]pyridin-4-amine
Bernardino, Alice M. R.
Pinheiro, Luiz C. S.
Tiekink, Edward R. T.
Wardell, James L.
Wardell, Solange M. S. V.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O2135 - +
[30] 4-ethyl-2,3-dihydro-4H-pyrido[3,2-e]-1,2,4-thiadiazine 1,1-dioxide and 4-ethyl-2,3-dihydro-4H-pyrido[4,3-e]-1,2,4-thiadiazine 1,1-dioxide
Dupont, L
Pirotte, B
Podona, T
Diouf, O
Delarge, J
De Tullio, P
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1999, 55 : 461 - 464

← 1 2 3 4 5 →