Hybrid microwave/conventionally heated calorimeter

被引：5
|
作者：
Binner, JGP
Price, DM [1 ]
Reading, M
Vaidhyanathan, B
机构：
[1] Univ Loughborough, Inst Polymer Technol & Mat Engn, Loughborough LE11 3TU, Leics, England
[2] Univ E Anglia, Dept Chem Sci & Pharm, Norwich NR4 7TJ, Norfolk, England
来源：
REVIEW OF SCIENTIFIC INSTRUMENTS | 2005年 / 76卷 / 06期
关键词：
D O I：
10.1063/1.1938787
中图分类号：
TH7 [仪器、仪表];
学科分类号：
0804 ; 080401 ; 081102 ;
摘要：
The design and construction of a calorimeter in which the specimen may be heated by microwave radiation and/or hot air is described. The apparatus was used to examine the effect of microwave radiation on the melting of benzil (89 degrees C) and the solid-state phase transition of silver iodide (147 degrees C). Reproducibility of transition temperature determinations were within +/- 1 degrees C. No changes were observed for benzil but silver iodide exhibited an apparent reduction in transition temperature to around 120 degrees C in the presence of microwaves, which increased with the level of microwave irradiation. (c) 2005 American Institute of Physics.
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页数：4
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