Gas-Chromatographic Identification of Chloro- and Bromo-Substituted Anilines by Their Retention Indices

被引：1
|
作者：
Gruzdev, I. V. [1 ]
Alferova, M. V. [2 ]
Kondratenok, B. M. [1 ]
Zenkevich, I. G. [3 ]
机构：
[1] Russian Acad Sci, Inst Biol, Komi Sci Ctr, Ural Branch, Syktyvkar 167982, Russia
[2] Syktyvkar State Univ, Dept Biol & Chem, Syktyvkar 167005, Russia
[3] St Petersburg State Univ, Dept Chem, St Petersburg 198504, Russia
来源：
JOURNAL OF ANALYTICAL CHEMISTRY | 2011年 / 66卷 / 05期
关键词：
chloroanilines; bromo-derivatives of chloroanilines; capillary gas chromatography; gas chromatography retention indices; SOLID-PHASE EXTRACTION; NON-POLAR COLUMN; AROMATIC-AMINES; MASS-SPECTROMETRY; WATER SAMPLES; DERIVATIZATION; BROMINATION; PHENOLS; MICROEXTRACTION; DERIVATIVES;
D O I：
10.1134/S1061934811050054
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Gas chromatography retention indices were experimentally determined for 27 chloro- and bromo-substituted anilines on the standard non-polar polydimethylsiloxane stationary phase; a procedure for the estimation of retention indices for any other species of the studied class was proposed. The computational algorithm is based on a modified additive scheme equivalent to the assembly of the target structure from simpler molecules characterized by retention indices, using their addition and subtraction.
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页码：504 / 509
页数：6
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