Gas-Chromatographic Identification of Chloro- and Bromo-Substituted Anilines by Their Retention Indices

被引：1

作者：

Gruzdev, I. V. ^{[1
]}

Alferova, M. V. ^{[2
]}

Kondratenok, B. M. ^{[1
]}

Zenkevich, I. G. ^{[3
]}

机构：

[1] Russian Acad Sci, Inst Biol, Komi Sci Ctr, Ural Branch, Syktyvkar 167982, Russia

[2] Syktyvkar State Univ, Dept Biol & Chem, Syktyvkar 167005, Russia

[3] St Petersburg State Univ, Dept Chem, St Petersburg 198504, Russia

来源：

JOURNAL OF ANALYTICAL CHEMISTRY | 2011年 / 66卷 / 05期

关键词：

chloroanilines; bromo-derivatives of chloroanilines; capillary gas chromatography; gas chromatography retention indices; SOLID-PHASE EXTRACTION; NON-POLAR COLUMN; AROMATIC-AMINES; MASS-SPECTROMETRY; WATER SAMPLES; DERIVATIZATION; BROMINATION; PHENOLS; MICROEXTRACTION; DERIVATIVES;

D O I：

10.1134/S1061934811050054

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Gas chromatography retention indices were experimentally determined for 27 chloro- and bromo-substituted anilines on the standard non-polar polydimethylsiloxane stationary phase; a procedure for the estimation of retention indices for any other species of the studied class was proposed. The computational algorithm is based on a modified additive scheme equivalent to the assembly of the target structure from simpler molecules characterized by retention indices, using their addition and subtraction.

引用

页码：504 / 509

页数：6

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