Synthesis and spectroscopic studies of isosteviol-calix[4]arene and -calix[6]arene conjugates

被引：28

作者：

Korochkina, M

Fontanella, M

Casnati, A ^{[1
]}

Arduini, A

Sansone, F

Ungaro, R

Latypov, S

Kataev, V

Alfonsov, V

机构：

[1] Univ Parma, Dipartimento Chim Organ & Ind, Parco Area Sci 17-A, I-43100 Parma, Italy

[2] AE Arbuzov Inst Organ & Phys Chem, Kazan 420088, Russia

来源：

TETRAHEDRON | 2005年 / 61卷 / 23期

基金：

俄罗斯基础研究基金会;

关键词：

calixarenes; isosteviol; NMR spectroscopy; molecular modelling; ab initio calculations;

D O I：

10.1016/j.tet.2005.03.127

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Novel calix[4]arene derivatives functionalized with two or four isosteviol units at the upper rim and a new calix[6]arene having six isosteviol moieties at the lower run have been synthesized. The structures of these compounds have been confirmed by NMR and mass spectrometry data. All H-1 and C-13 NMR chemical shifts of isosteviol were fully assigned by extensive NMR spectroscopic methods, and used to clarify the structures and conformations of isosteviol-calixarene, conjuates. (c) 2005 Elsevier Ltd. All rights reserved.

引用

页码：5457 / 5463

页数：7

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