2-[3-Hydroxy-4-(2-hydroxyethoxy)-phenyl]-4,4,5,5-tetramethyl-2-imidazoline-1-oxyl 3-oxide

被引：0
|
作者：
Ma, Hui-Ping [1 ]
Jing, Lin-Lin [1 ]
He, Lei [1 ]
Fan, Peng-Cheng [1 ]
Jia, Zheng-Ping [1 ]
机构：
[1] PLA, Dept Pharm, Lanzhou Gen Hosp, Key Lab Prevent & Cure Plateau Environm Damage, Lanzhou 730050, Gansu, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2012年 / 68卷
关键词：
Data-to-parameter ratio = 13.5; Mean σ(C-C) = 0.003 Å; R factor = 0.038; Single-crystal X-ray study; T = 296 K; wR factor = 0.103;
D O I：
10.1107/S1600536811053979
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C15H21N2O5, the imidazoline ring displays a twisted conformation. The mean plane of the imidazoline ring makes a dihedral angle of 22.55 (5)degrees with the benzene ring. In the crystal, O-H center dot center dot center dot O and C-H center dot center dot center dot O hydrogen bonds link the molecules into a layer parallel to the bc plane.
引用
收藏
页数：9
相关论文
共 50 条
  • [31] Preparation and property of 2-(3',5'-di-tert-butylphenyl-4'-oxyl)-4,4,5,5-tetramethyl-4,5, dihydro-1H-imidazole-3-oxide-1-oxyl
    Ishiguro, K
    Ozaki, M
    Kamekura, Y
    Sekine, N
    Sawaki, Y
    MOLECULAR CRYSTALS AND LIQUID CRYSTALS SCIENCE AND TECHNOLOGY SECTION A-MOLECULAR CRYSTALS AND LIQUID CRYSTALS, 1997, 306 : 75 - 80
  • [32] catena-Poly[[diaquacobalt(II)]bis[μ-2-(4-carboxylatophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazol-1-oxyl 3-oxide]]
    Rong, Rong
    Gao, Ge
    Zhu, Lili
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : M488 - U923
  • [33] SYNTHESIS AND CHARACTERIZATION OF 2-FERROCENYL-4,4,5,5-TETRAMETHYL-2-IMIDAZOLIN-1-OXYL 3-OXIDE AND ITS CT-COMPLEX WITH DDQ
    NAKAMURA, Y
    KOGA, N
    IWAMURA, H
    CHEMISTRY LETTERS, 1991, (01) : 69 - 72
  • [34] Diazidobis[4,4,5,5-tetramethyl-2-(1,3-thiazol-2-yl)-2-imidazoline-1-oxyl-3-oxide-κ2O,N]manganese(II)
    Chang, Jiu Li
    Gao, Zhi Yong
    Jiang, Kai
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M181 - U609
  • [35] Structure of 2,4,4,5,5-pentamethyl-2-imidazoline-1-oxyl-3-oxide
    Romanenko, GV
    Ovcharenko, DV
    Vasilevskii, SF
    JOURNAL OF STRUCTURAL CHEMISTRY, 2003, 44 (02) : 314 - 317
  • [36] Spin transition in the molecular heterospin complex of Cu(hfac)2 with 4,4,5,5-tetramethyl-2-(1-methylpyrazol-5-yl)-4,5-dihydroimidazole-1-oxyl 3-oxide
    S. V. Fokin
    E. T. Kostina
    E. V. Tret’yakov
    G. V. Romanenko
    A. S. Bogomyakov
    R. Z. Sagdeev
    V. I. Ovcharenko
    Russian Chemical Bulletin, 2013, 62 : 661 - 671
  • [37] 4,4,5,5-tetramethyl-2-(4-pyridyl)-imidazolidin-1-oxyl-3-oxide trichloroacetic acid solvate
    Chen, Hong-Xian
    Li, Zhong-Shu
    Sun, Bai-Wang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1197 - U1276
  • [38] Spin transition in the molecular heterospin complex of Cu(hfac)2 with 4,4,5,5-tetramethyl-2-(1-methylpyrazol-5-yl)-4,5-dihydroimidazole-1-oxyl 3-oxide
    Fokin, S. V.
    Kostina, E. T.
    Tret'yakov, E. V.
    Romanenko, G. V.
    Bogomyakov, A. S.
    Sagdeev, R. Z.
    Ovcharenko, V. I.
    RUSSIAN CHEMICAL BULLETIN, 2013, 62 (03) : 661 - 671
  • [39] Dichloridobis[4,4,5,5-tetramethyl-2-(5-methyl-1H-imidazol-4-yl-κN3)-2-imidazoline-1-oxyl 3-oxide-κO]copper(II)
    Gao, Zhi Yong
    Zhang, Wen Bei
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : M1504 - +
  • [40] (R)-2-[1-(2,6-Dichloro-3,4,5-trimethoxybenzoyl)pyrrolidin-2-yl]-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazole-1-oxyl 3-oxide
    Wang, Hai-Bo
    Xiang, Zhuo
    Jing, Lin-Lin
    Tian, Min
    Sun, Xiao-Li
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O985 - U1492
12345