2-[3-Hydroxy-4-(2-hydroxyethoxy)-phenyl]-4,4,5,5-tetramethyl-2-imidazoline-1-oxyl 3-oxide

被引：0
|
作者：
Ma, Hui-Ping [1 ]
Jing, Lin-Lin [1 ]
He, Lei [1 ]
Fan, Peng-Cheng [1 ]
Jia, Zheng-Ping [1 ]
机构：
[1] PLA, Dept Pharm, Lanzhou Gen Hosp, Key Lab Prevent & Cure Plateau Environm Damage, Lanzhou 730050, Gansu, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2012年 / 68卷
关键词：
Data-to-parameter ratio = 13.5; Mean σ(C-C) = 0.003 Å; R factor = 0.038; Single-crystal X-ray study; T = 296 K; wR factor = 0.103;
D O I：
10.1107/S1600536811053979
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C15H21N2O5, the imidazoline ring displays a twisted conformation. The mean plane of the imidazoline ring makes a dihedral angle of 22.55 (5)degrees with the benzene ring. In the crystal, O-H center dot center dot center dot O and C-H center dot center dot center dot O hydrogen bonds link the molecules into a layer parallel to the bc plane.
引用
收藏
页数：9
相关论文
共 50 条
  • [21] Seven-membered metallocycle in the CuII complex with deprotonated 2-(2-hydroxy-3-nitrophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazole-1-oxyl 3-oxide
    Petrov, PA
    Tret'yakov, EV
    Romanenko, GV
    Ovcharenko, VI
    Sagdeev, RZ
    RUSSIAN CHEMICAL BULLETIN, 2004, 53 (01) : 109 - 113
  • [22] Seven-membered metallocycle in the CuII complex with deprotonated 2-(2-hydroxy-3-nitrophenyl)-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazole-1-oxyl 3-oxide
    P. A. Petrov
    E. V. Tret"yakov
    G. V. Romanenko
    V. I. Ovcharenko
    R. Z. Sagdeev
    Russian Chemical Bulletin, 2004, 53 : 109 - 113
  • [23] Structure and magnetic properties of the stable nitroxide 2-cyano-4,4,5,5-tetramethyl-3-oxide-2-imidazoline-1-oxyl
    Koreneva, OV
    Romanenko, GV
    Ikorskii, VN
    Fokin, SV
    Ovcharenko, VI
    JOURNAL OF STRUCTURAL CHEMISTRY, 2001, 42 (05) : 820 - 825
  • [24] Diaqua(3,5-dinitrobenzoato)bis[4,4,5,5-tetramethyl-2-(4-pyridyl)imidazolin-1-oxyl 3-oxide]copper(II)
    Zhang, Chen-Xi
    An, Li-Juan
    Sun, Dong-Lan
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : M3345 - M3346
  • [25] Dimethanolbis[4,4,5,5-tetramethyl-2-(5-methylimidazol-4-yl)-2-imidazoline-1-oxyl-3-oxide-κ2O,N]cobalt(II)diperchlorate
    Gao, Zhi Yong
    Guo, Hua Jie
    Zhang, Wen Bei
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M19 - U297
  • [26] Structure of 2,4,4,5,5‐pentamethyl‐2‐imidazoline‐1‐oxyl‐3‐oxide
    G. V. Romanenko
    D. V. Ovcharenko
    S. F. Vasilevskii
    Journal of Structural Chemistry, 2003, 44 : 314 - 317
  • [27] Diaquabis(benzoato-kappa O)bis[4,4,5,5-tetramethyl-2-(pyridin-4-yl-kappa N)-imidazoline-1-oxyl 3-oxide]cobalt(II)
    Wang, Kun-Miao
    Zhou, Jie
    Qian, Fen-Hua
    Liu, Jing
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : M506 - +
  • [28] 2-[1-(tert-Butoxycarbonyl)pyrrolidin-2-yl]-4,4,5,5-tetramethyl-4,5-dihydro-1H-imidazole-1-oxyl 3-oxide
    Jiang, Ru
    Wang, Hai-Bo
    Gao, Peng
    Jing, Lin-Lin
    Sun, Xiao-Li
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1954 - U649
  • [29] 2-[1-(4-Chlorobenzoyl)pyrrolidin-2-yl]-4,4,5,5-tetramethyl-4,5-dihydroimidazole-1-oxyl-3-oxide
    Tian, Min
    Xiang, Zhuo
    Zhou, Si-Yuan
    Jing, Lin-Lin
    Wang, Hai-Bo
    Sun, Xiao-Li
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O425 - U1154
  • [30] Preparation and property of 2-(3′,5′-di-tert-butylphenyl -4′-oxyl)-4,4,5,5-tetramethyl-4,5,-dihydro-1H-imidazole-3-oxide-1-oxyl
    Ishiguro, Katsuya
    Ozaki, Mitsutoshi
    Kamekura, Yasuo
    Sekine, Nobuyuki
    Sawaki, Yasuhiko
    Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 1997, 306 : 75 - 80
12345