Room temperature synthesis and solid-state structure of Ni2P2O6 • 12H2O

被引：14
|
作者：
Haag, JM
LeBret, GC
Cleary, DA
Twamley, B
机构：
[1] Gonzaga Univ, Dept Chem, Spokane, WA 99258 USA
[2] Univ Idaho, Univ Res Off, Moscow, ID 83844 USA
来源：
JOURNAL OF SOLID STATE CHEMISTRY | 2005年 / 178卷 / 04期
基金：
美国国家科学基金会;
关键词：
metal hypodiphosphate; room temperature synthesis;
D O I：
10.1016/j.jssc.2004.12.005
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The synthesis and crystal structure of Ni2P2O6 center dot 12H(2)O are reported. The compound was synthesized from aqueous solutions of nickel chloride and sodium hypodiphosphate at room temperature. The space group is orthorhombic, Pnnm. Unit cell dimensions are a = 11.2418(5) angstrom, b = 18.5245(8) angstrom, and c = 7.3188(3) angstrom, Z = 4. The product is unstable with respect to dehydration above room temperature. (c) 2004 Elsevier Inc. All rights reserved.
引用
收藏
页码：1308 / 1311
页数：4
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