Room temperature synthesis and solid-state structure of Ni2P2O6 • 12H2O

被引：14
|
作者：
Haag, JM
LeBret, GC
Cleary, DA
Twamley, B
机构：
[1] Gonzaga Univ, Dept Chem, Spokane, WA 99258 USA
[2] Univ Idaho, Univ Res Off, Moscow, ID 83844 USA
来源：
JOURNAL OF SOLID STATE CHEMISTRY | 2005年 / 178卷 / 04期
基金：
美国国家科学基金会;
关键词：
metal hypodiphosphate; room temperature synthesis;
D O I：
10.1016/j.jssc.2004.12.005
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The synthesis and crystal structure of Ni2P2O6 center dot 12H(2)O are reported. The compound was synthesized from aqueous solutions of nickel chloride and sodium hypodiphosphate at room temperature. The space group is orthorhombic, Pnnm. Unit cell dimensions are a = 11.2418(5) angstrom, b = 18.5245(8) angstrom, and c = 7.3188(3) angstrom, Z = 4. The product is unstable with respect to dehydration above room temperature. (c) 2004 Elsevier Inc. All rights reserved.
引用
收藏
页码：1308 / 1311
页数：4
相关论文
共 50 条
  • [31] Simple Preparation, Structure and Conductivity of Nickel(II) Benzenetricarboxylate Ni3(BTC)2•12H2O
    Tan Hai-Yan
    Liu Cheng
    Wang Zhao-Hui
    Wu Jin-Ping
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2014, 33 (03) : 401 - 406
  • [32] Synthesis, characterization and solid-state properties of [Zn(Hdmmthiol)2]•2H2O complex
    Dagdelen, Fethi
    Aydogdu, Yildirim
    Dey, Kamalendu
    Biswas, Susobhan
    EUROPEAN PHYSICAL JOURNAL PLUS, 2016, 131 (05):
  • [33] SYNTHESIS AND STRUCTURE OF K6ZR12(O2)3.2H2O.2H2O POLYNUCLEAR PEROXOFLUOROZIRCONATES
    CHERNYSHOV, BN
    DIDENKO, NA
    BUKVETSKII, BV
    GERASIMENKO, AV
    KAVUN, VY
    SERGIENKO, SS
    ZHURNAL NEORGANICHESKOI KHIMII, 1989, 34 (11): : 2786 - 2794
  • [34] THE STRUCTURE OF HEXAPOTASSIUM DISODIUM HEXATUNGSTOPLATINATE(IV) DODECAHYDRATE, K6NA2[PTW6O24].12H2O
    LEE, U
    ICHIDA, H
    KOBAYASHI, A
    SASAKI, Y
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1984, 40 (JAN) : 5 - 7
  • [35] Synthesis and Photocatalytic Properties of a New Heteropolyoxoniobate Compound: K10[Nb2O2(H2O)2][SiNb12O40]•12H2O
    Zhang, Zhenyu
    Lin, Qipu
    Kurunthu, Dharmalingam
    Wu, Tao
    Zuo, Fan
    Zheng, Shou-Tian
    Bardeen, Christopher J.
    Bu, Xianhui
    Feng, Pingyun
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2011, 133 (18) : 6934 - 6937
  • [36] Ni2CdCl6·12H2O中Ni2+离子的光谱及其局域结构研究
    冯文林
    谌家军
    量子电子学报, 2007, (02) : 142 - 145
  • [37] Synthesis and crystal structure of [Ni(H2O)6] (C19H17O9S)2•2H2O
    Zhang, Zun-Ting
    Zhang, Xue-Ling
    Zhang, Yun He
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2006, 36 (08) : 517 - 522
  • [38] Synthesis and crystal structure of [Ni(H2O)6](C19H17O9S)2·2H2O
    Zun-Ting Zhang
    Xue-Ling Zhang
    Yun He
    Journal of Chemical Crystallography, 2006, 36 : 517 - 522
  • [39] Synthesis and Crystal Structure of an Ionic Compound [Fe（CN）6·（PhCH2NC9H7）4]·12H2O
    黄华鸣
    边秀珠
    杜巧云
    Chinese Journal of Structural Chemistry, 2009, (07) : 859 - 863
  • [40] Synthesis and Crystal Structure of an Ionic Compound [Fe(CN)6•(PhCH2NC9H7)4]•12H2O
    Huang Hua-Ming
    Bian Xiu-Zhu
    Du Qiao-Yun
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2009, 28 (07) : 859 - 863
12345