Unusual peptides containing the 2,6-diaminopimelic acid framework: Stereocontrolled synthesis, X-ray analysis, and computational modelling. Part 2

被引：19

作者：

Galeazzi, R

Garavelli, M

Grandi, A

Monari, M

Porzi, G

Sandri, S

机构：

[1] Univ Bologna, Dipartimento Chim G Ciamician, I-40126 Bologna, Italy

[2] Univ Ancona, Dipartimento Sci Mat & Terra, I-60131 Ancona, Italy

来源：

TETRAHEDRON-ASYMMETRY | 2003年 / 14卷 / 17期

关键词：

D O I：

10.1016/S0957-4166(03)00541-X

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The stereocontrolled synthesis of peptides 6, 9 and 14, structural variants of 2,6-diaminopimelic acid, was carried out starting from the chiral synthon 1. easily obtained from L-valine. The configuration of the introduced stereogenic centres has been assigned on the basis of H-1 NMR spectroscopic data. X-Ray crystal structure and conformation analysis of 5 are also reported. (C) 2003 Elsevier Ltd. All rights reserved.

引用

页码：2639 / 2649

页数：11

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