Solvent-free mechanochemical and liquid-phase reaction of [60]fullerene with ethyl 2-diazopropionate

被引：0
|
作者：
Li, YJ
Peng, RF
Liu, YC
Wang, GW [1 ]
机构：
[1] Lanzhou Univ, State Key Lab Appl Organ Chem, Lanzhou 730000, Peoples R China
[2] Univ Sci & Technol China, Dept Chem, Anhua 230026, Peoples R China
来源：
CHINESE CHEMICAL LETTERS | 2004年 / 15卷 / 11期
关键词：
60]fullerene; ethyl; 2-diazopropionate; methanofullerene; fulleroid;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The solvent-free mechanochemical reaction and the liquid-phase reaction of C-60 with ethyl 2-diazopropionate prepared in situ or preformed from alanine ethyl ester hydrochloride and sodium nitrite have been investigated. Methanofullerene 1 and fulleroids 2 and 3 from these reactions were obtained, meanwhile the pyrazoline intermediate was not observed. Fulleroids 2 and 3 can be converted to methanofullerene 1 in refluxing toluene.
引用
收藏
页码：1265 / 1268
页数：4
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