Solvent-free Synthesis of Dihydrofuran-fused [60]Fullerene Derivatives by High-speed Vibration Milling

被引：0
|
作者：
Yasujiro MURATA
Koichi KOMATSU
机构：
[1] Institute for Chemical Research
[2] Japan
[3] Kyoto 611-0011
[4] Kyoto University
[5] Uji
来源：
ChineseChemicalLetters | 2005年 / 10期
关键词：
60]Fullerene; mechanochemical; solvent-free; β-dicarbonyl compounds;
D O I：
暂无
中图分类号：
O621.2 [有机化合物性质];
学科分类号：
070303 ; 081704 ;
摘要：
Solvent-free reactions of 1, 3-cyclohexanedione, 5, 5-dimethyl-1, 3-cyclohexanedione, 2, 4-pentanedione and ethyl acetoacetate with C60 in the presence of Mn(OAc)3·2H2O and ceric ammonium nitrate (CAN) under the high-speed vibration milling conditions afforded dihydrofuran-fused C60 derivatives. CAN is the better oxidant than Mn(OAc)3·2H2O in these mechanochemical reactions.
引用
收藏
页码：1327 / 1329
页数：3
相关论文
共 50 条
  • [1] Solvent-free synthesis of dihydrofuran-fused [60]fullerene derivatives by high-speed vibration milling
    Cheng, X
    Wang, GW
    Murata, Y
    Komatsu, K
    CHINESE CHEMICAL LETTERS, 2005, 16 (10) : 1327 - 1329
  • [2] Palladium-Catalyzed Synthesis of Dihydrofuran-Fused [60]Fullerene Derivatives via Heteroannulation of Olefins
    Zhu, San'e
    Dou, Lifeng
    Zhang, Jianhui
    Wu, Ying
    Yang, Wei
    Lu, Hongdian
    Wei, Chunxiang
    Deng, Chonghai
    Dong, Qiang
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2021, 41 (05) : 2082 - 2090
  • [3] Solvent-free synthesis of 2-aminothiophene-3-carbonitrile derivatives using high-speed vibration milling
    Xu, Fang
    Li, Yujin
    Xu, Fengshuang
    Ye, Qing
    Han, Liang
    Gao, Jianrong
    Yu, Wubin
    JOURNAL OF CHEMICAL RESEARCH, 2014, (07) : 450 - 452
  • [4] Solvent-free self-assembly of C60 and cucurbit[7]uril using high-speed vibration milling
    Constabel, F
    Geckeler, KE
    TETRAHEDRON LETTERS, 2004, 45 (10) : 2071 - 2073
  • [5] Broad Synthesis of Disubstituted Dihydrofuran-Fused [60]Fullerene Derivatives via Cu(I)/Ag(I)-Mediated Synergistic Annulation Reaction
    Xia, Shilu
    Liu, Tong-Xin
    Zhang, Pengling
    Ma, Jinliang
    Liu, Qingfeng
    Ma, Nana
    Zhang, Zhiguo
    Zhang, Guisheng
    JOURNAL OF ORGANIC CHEMISTRY, 2018, 83 (02): : 862 - 870
  • [6] Solvent-free reactions of fullerenes and N-alkylglycines with and without aldehydes under high-speed vibration milling
    Wang, GW
    Zhang, TH
    Hao, EH
    Jiao, LJ
    Murata, Y
    Komatsu, K
    TETRAHEDRON, 2003, 59 (01) : 55 - 60
  • [7] SYNTHESIS OF QUINOLINES BY N-DEFORMYLATION AND AROMATIZATION VIA SOLVENT-FREE, HIGH-SPEED BALL MILLING
    Yu, Jingbo
    Li, Zhenhua
    Su, Weike
    SYNTHETIC COMMUNICATIONS, 2013, 43 (03) : 361 - 374
  • [8] Solvent-free reactions of fullerenes with diethyl bromomalonate in the presence of inorganic bases under high-speed vibration milling conditions
    Peng, RF
    Wang, GW
    Shen, YB
    Li, YJ
    Zhang, TH
    Liu, YC
    Murata, Y
    Komatsu, K
    SYNTHETIC COMMUNICATIONS, 2004, 34 (11) : 2117 - 2126
  • [9] Solvent-Free Synthesis of β-Enamino Ketones (Esters) under High-Speed Vibration Miling (HSVM) Condition
    Fan, Wenming
    Gao, Jianrong
    Jia, Jianhong
    Han, Liang
    Sheng, Weijian
    Li, Yujin
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2010, 30 (11) : 1732 - 1736
  • [10] Solvent and catalyst free azo-Michael addition under high-speed vibration milling
    YuJin Li
    YongWen Cao
    FengShuang Xu
    WenMing Fang
    WuBin Yu
    JianHong Jia
    JianRong Gao
    Science China Chemistry, 2012, 55 : 1252 - 1256
12345