The influence of ethylene glycol on the preparation of K2SnSi3O9•H2O

被引：0
|
作者：
Lin, Zhi [1 ]
机构：
[1] Univ Aveiro, Dept Chem, CICECO, P-3810193 Aveiro, Portugal
来源：
ZEOLITES AND RELATED MATERIALS: TRENDS, TARGETS AND CHALLENGES, PROCEEDINGS OF THE 4TH INTERNATIONAL FEZA CONFERENCE | 2008年 / 174卷
关键词：
Silicate; stannosilicate; solvothermal synthesis;
D O I：
暂无
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
The influence of ethylene glycol (EG) on the preparation of K(2)SnSi(3)O(9)center dot H(2)O (AV-6) was studied in this work. The EG content clearly changes the synthesis process. Although the morphology of the samples is similar, the products are mixtures containing AV-6, AV-7 (K(2)SnSi(3)O(9)center dot H(2)O) and AV-11 (K(4)Sn(2)Si(6)O(18)). At high EG content, nano crystal of Sn-AV-11, instead of AV-6, is crystallized from the system. The samples were characterized by powder XRD, SEM, solid-state (29)Si MAS NMR spectroscopy and thermogravimetric (TG) analysis.
引用
收藏
页码：301 / 304
页数：4
相关论文
共 50 条
  • [41] K3H2P3O10-CO(NH2)-H2O SYSTEM
    NABIEV, MN
    NAMAZOV, SS
    YANTSIEVA, SK
    TUKHTAEV, S
    KUCHAROV, K
    ZHURNAL NEORGANICHESKOI KHIMII, 1987, 32 (01): : 250 - 252
  • [42] Influence of H2O and H2S on the composition, activity, and stability of sulfided Mo, CoMo, and NiMo supported on MgAl2O4 for hydrodeoxygenation of ethylene glycol
    Dabros, Trine Marie Hartmann
    Gaur, Abhijeet
    Pintos, Delfina Garcia
    Sprenger, Paul
    Hoj, Martin
    Hansen, Thomas Willum
    Studt, Felix
    Gabrielsen, Jostein
    Grunwaldt, Jan-Dierk
    Jensen, Anker Degn
    APPLIED CATALYSIS A-GENERAL, 2018, 551 : 106 - 121
  • [43] KINETIC-STUDIES ON THE NCS- SUBSTITUTION OF H2O ON 2 INCOMPLETE CUBOIDAL W(IV)3 COMPLEXES - [W3O2S2(H2O)9]4+ AND [W3OS3(H2O)9]4+
    LI, YJ
    ROUTLEDGE, CA
    SYKES, AG
    INORGANIC CHEMISTRY, 1991, 30 (26) : 5043 - 5046
  • [44] Preparation and characterization of heteropoly compound Mn3[Zr(H2O)CoW9Mo2O39]•21H2O
    Wu, QY
    Sang, XG
    He, YC
    Li, X
    MATERIALS LETTERS, 2003, 57 (24-25) : 4028 - 4032
  • [45] Investigation of the ion-exchanged forms of the microporous titanosilicate K2TiSi3O9•H2O
    Valtchev, V
    Paillaud, JL
    Mintova, S
    Kessler, H
    MICROPOROUS AND MESOPOROUS MATERIALS, 1999, 32 (03) : 287 - 296
  • [46] SynthesisandCrystalStructureof（H3O）2[Cu3Cl3（H2O）3(NC9H12.5O6)2]
    ZHANG RuiBo ZHANG Jian WEN YiHang CHENG JianKai LI ZhaoJi YAO YuanGen State Key Laboratory of Structural Chemistry Fujian Institute of Research on the Structure of Matter The Chinese Academy of Sciences Fuzhou Fujian China
    结构化学, 2005, (11)
  • [47] Y(HSeO3)(SeO3)(H2O)]•H2O
    Harrison, William T. A.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : I152 - I154
  • [48] Temperature Dependence of Vapor Pressures over Saturated Aqueous Solutions at Invariant Points of the NaCl + KCl + H2O, NaCl + NaNO3 + H2O, KCl + KBr + H2O, KCl + KI + H2O, KCl + KNO3 + H2O, and KCl + K2SO4 + H2O Systems
    Apelblat, Alexander
    Korin, Eli
    JOURNAL OF CHEMICAL AND ENGINEERING DATA, 2009, 54 (05): : 1619 - 1624
  • [49] Supramolecular Coordination Assemblies Using 2-Aminodiacetic Terephthalic Acid Ligands: K[NiII(Hadta)(H2O)2]·H2O and K[Cu1.5II(adta)(H2O)1.5]·H2O
    David P. Walsh
    Lei Zhang
    Paul E. Kruger
    Wolfgang Schmitt
    Journal of Inorganic and Organometallic Polymers and Materials, 2011, 21
  • [50] Phase equilibria of AlCl3 + FeCl3 + H2O, AlCl3 + CaCl2 + H2O, and FeCl3 + CaCl2 + H2O at 298.15 K
    Yuan, Mengxia
    Qiao, Xiuchen
    Yu, Jianguo
    JOURNAL OF CHEMICAL AND ENGINEERING DATA, 2016, 61 (05): : 1749 - 1755
12345