The influence of ethylene glycol on the preparation of K2SnSi3O9•H2O

被引：0
|
作者：
Lin, Zhi [1 ]
机构：
[1] Univ Aveiro, Dept Chem, CICECO, P-3810193 Aveiro, Portugal
来源：
ZEOLITES AND RELATED MATERIALS: TRENDS, TARGETS AND CHALLENGES, PROCEEDINGS OF THE 4TH INTERNATIONAL FEZA CONFERENCE | 2008年 / 174卷
关键词：
Silicate; stannosilicate; solvothermal synthesis;
D O I：
暂无
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
The influence of ethylene glycol (EG) on the preparation of K(2)SnSi(3)O(9)center dot H(2)O (AV-6) was studied in this work. The EG content clearly changes the synthesis process. Although the morphology of the samples is similar, the products are mixtures containing AV-6, AV-7 (K(2)SnSi(3)O(9)center dot H(2)O) and AV-11 (K(4)Sn(2)Si(6)O(18)). At high EG content, nano crystal of Sn-AV-11, instead of AV-6, is crystallized from the system. The samples were characterized by powder XRD, SEM, solid-state (29)Si MAS NMR spectroscopy and thermogravimetric (TG) analysis.
引用
收藏
页码：301 / 304
页数：4
相关论文
共 50 条
  • [21] H2O2 photoproduction inside H2O and H2O:O2 ices at 20-140 K
    Kulikov, Mikhail Yu
    Feigin, Alexander M.
    Schrems, Otto
    SCIENTIFIC REPORTS, 2019, 9 (1)
  • [22] SYNCHROTRON RADIATION MEASUREMENTS OF APPEARANCE POTENTIALS FOR (H2O)2+, (H2O)3+, (H2O)H-2(+) AND (H2O)H-3(+) IN SUPERSONIC JETS
    SHIROMARU, H
    SHINOHARA, H
    WASHIDA, N
    YOO, HS
    KIMURA, K
    CHEMICAL PHYSICS LETTERS, 1987, 141 (1-2) : 7 - 11
  • [23] CRYSTAL-STRUCTURE OF (NME4)2[RE3BR11(H2O)][RE3BR9(H2O)3](H2O)2
    MOLLER, A
    MEYER, G
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1993, 619 (10): : 1655 - 1660
  • [24] PREPARATION AND CRYSTALLOGRAPHIC STUDY OF A CYCLOTRIPHOSPHATE SERIES - SMNA3(P3O9)2, 9H2O, EUNA3(P3O9)2, 9H2O, GDNA3(P3O9)2, 9H2O, DYNA3(P3O9)2, 9H2O, HONA3(P3O9)2, 9H2O, ERNA3(P3O9)2, 9H2O, YNA3(P3O9)2, 9H2O
    BAGIEUBEUCHER, M
    COMPTES RENDUS DE L ACADEMIE DES SCIENCES SERIE II, 1989, 308 (04): : 377 - 379
  • [25] Syntheses and structures of seven-coordinate K3[Cd(Dtpa)], K2[Cd(H2O)4][Cd(Edta)(H2O)]2 · 2H2O, and Na2[Cd(H2O)4][Cd(Edta)(H2O)]2 · 2H2O complexes
    X. F. Wang
    Y. F. Wang
    J. Wang
    Zh. H. Zhang
    J. Gao
    B. Liu
    Y. Ch. Jiang
    X. D. Zhang
    Russian Journal of Coordination Chemistry, 2008, 34 : 555 - 563
  • [26] Syntheses and structures of seven-coordinate K3[Cd(Dtpa)], K2[Cd(H2O)4][Cd(Edta)(H2O)]2 • 2H2O, and Na2[Cd(H2O)4][Cd(Edta)(H2O)]2 • 2H2O complexes
    Wang, X. F.
    Wang, Y. F.
    Wang, J.
    Zhang, Zh. H.
    Gao, J.
    Liu, B.
    Jiang, Y. Ch.
    Zhang, X. D.
    RUSSIAN JOURNAL OF COORDINATION CHEMISTRY, 2008, 34 (08) : 555 - 563
  • [27] INFRARED-SPECTRA OF THE HYDRATED HYDRONIUM IONS, H3O(H2O)1+, H3O(H2O)2+, H3O(H2O)3+
    YEH, LI
    OKUMURA, M
    MYERS, JD
    LEE, YT
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1987, 193 : 170 - PHYS
  • [28] Synthesis and crystal structures of [K(H2O)(Piv)]∞ and [K2(Phen)(H2O)2(Piv)2]∞
    D. M. Tsymbarenko
    E. A. Bukhtoyarova
    I. E. Korsakov
    S. I. Troyanov
    Russian Journal of Coordination Chemistry, 2011, 37 : 825 - 831
  • [29] Synthesis and Crystal Structures of [K(H2O)(Piv)]∞ and [K2(Phen)(H2O)2(Piv)2]∞
    Tsymbarenko, D. M.
    Bukhtoyarova, E. A.
    Korsakov, I. E.
    Troyanov, S. I.
    RUSSIAN JOURNAL OF COORDINATION CHEMISTRY, 2011, 37 (11) : 825 - 831
  • [30] Vajdakite (MoO2)2(H2O)2AS3+2O5•H2O
    不详
    CANADIAN MINERALOGIST, 2003, 41 : 1318 - 1318
12345