1-{1-[(2-Chlorothiazol-5-yl)methyl]2-[(2-chlorothiazol-5-yl)methylsulfanyl]-4-methyl-6-phenyl-1,6-dihydropyrimidin-5-yl}ethanone

被引:0
|
作者
Xiao-Fei Zhu [1 ]
De-Qing Shi [1 ]
Fang Luo [1 ]
Zhi-Fang Wang [1 ]
机构
[1] Cent China Normal Univ, Coll Chem, Key Lab Pesticides & Chem Biol, Wuhan 430079, Peoples R China
关键词
D O I
10.1107/S1600536807033764
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The crystal structure of the title compound, C21H18Cl2N4OS3, is stabilized by intermolecular C-H center dot center dot center dot O and C-H center dot center dot center dot N hydrogen bonds. The dihydropyrimidine ring is almost planer, with a mean deviation from the plane of 0.132 (1) angstrom. The dihedral angles between the dihydropyrimidine ring and the phenyl, 1-thiazole and 2-thiazole rings are 88.5 (1), 13.6 (1) and 8.0 (1)degrees, respectively.
引用
收藏
页码:O3516 / U3554
页数:11
相关论文
共 50 条
  • [31] 1-{5-Methyl-1-[8-(trifluoromethyl)-quinolin-4-yl]-1H-1,2,3-triazol-4-yl}-ethanone
    Thiruvalluvar, A.
    Subramanyam, M.
    Butcher, R. J.
    Mahalinga, M.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O4813 - U6034
  • [32] Novel 2-(benzo[d]thiazol-2-yl)-1-(3-methyl-5-substituted-phenyl-4,5-dihydropyrazol-1-yl)ethanone Derivatives: Synthesis and Antibacterial Activity
    Pan, Chun-Xiu
    Li, Jun
    Liu, Xin-Hua
    LETTERS IN DRUG DESIGN & DISCOVERY, 2011, 8 (05) : 459 - 463
  • [33] Synthesis and tautomerism of 2-[3(5)-aryl(methyl)pyrazol-4-yl]-1- benzimidazoles
    Dzvinchuk I.B.
    Lozinskii M.O.
    Chemistry of Heterocyclic Compounds, 2006, 42 (9) : 1190 - 1196
  • [34] N-[1-(1H-Benzimidazol-2-yl)-2-(5-chloro-3-methyl-1-phenyl-1H-pyrazol-4-yl)vinyl]benzamide
    Kaushik, Darpan
    Maan, Namita
    MOLBANK, 2011, (03)
  • [35] 1-[5-Methyl-1-(4-nitrophenyl)-1H-1,2,3-triazol-4-yl]ethanone
    Vinutha, N.
    Kumar, S. Madan
    Nithinchandrab
    Balakrishna, Kalluraya
    Lokanath, N. K.
    Revannasiddaiah, D.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1724 - +
  • [36] Synthesis and Structure of N-(4,6-dimethylpyrimidin-2-yl)-2-(5-phenyl-2H-tetrazol-2-yl)acetohydrazide and 1-(4,6-dimethylpyrimidin-2-yl)-3-[(5-phenyl-2H-tetrazol-2-yl)methyl]-1H-pyrazol-5-ol
    Nesterova, O. M.
    Zarubina, O. S.
    Tolstyakov, V. V.
    Danagulyan, G. G.
    Trifonov, R. E.
    Smirnov, S. N.
    Slepukhin, P. A.
    Ignatenko, N. K.
    Ostrovskii, V. A.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2017, 53 (11) : 1766 - 1768
  • [37] Synthesis and structure of N-(4,6-dimethylpyrimidin-2-yl)-2-(5-phenyl-2H-tetrazol-2-yl)acetohydrazide and 1-(4,6-dimethylpyrimidin-2-yl)-3-[(5-phenyl-2H-tetrazol-2-yl)methyl]-1H-pyrazol-5-ol
    O. M. Nesterova
    O. S. Zarubina
    V. V. Tolstyakov
    G. G. Danagulyan
    R. E. Trifonov
    S. N. Smirnov
    P. A. Slepukhin
    N. K. Ignatenko
    V. A. Ostrovskii
    Russian Journal of Organic Chemistry, 2017, 53 : 1766 - 1768
  • [38] 1-(1-Benzofuran-2-yl)-2-(phenylsulfonyl)ethanone
    Abdel-Aziz, Hatem A.
    Ng, Seik Weng
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2675 - +
  • [39] 1-(2-Methyl-5-nitro-1H-imidazol-1-yl)acetone
    Yousuf, Sammer
    Khan, Khalid M.
    Naz, Frazana
    Perveen, Shahanaz
    Miana, Ghulam A.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O552 - +
  • [40] 1-{1-[2,8-Bis(trifluoromethyl)-4-quinolyl]-5-methyl-1H-1,2,3-triazol-4-yl}ethanone
    Devarajegowda, H. C.
    Jeyaseelan, S.
    Sumangala, V.
    Bojapoojary
    Nayak, Suresh P.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2512 - U37