Synthesis of 1,8-dioxo-octahydroxanthenes utilizing nanodiatomite@melamine-SO3H as a novel heterogeneous catalyst under solvent-free conditions

被引：3

作者：

Davoodi, Elham ^{[1
,2
]}

Tahanpesar, Elham ^{[1
]}

Massah, Ahmad Reza ^{[3
]}

机构：

[1] Islamic Azad Univ, Dept Chem, Ahvaz Branch, Ahvaz, Iran

[2] Islamic Azad Univ, Dept Chem, Khuzestan Sci & Res Branch, Ahvaz, Iran

[3] Islamic Azad Univ, Dept Chem, Shahreza Branch, Esfahan 86145311, Iran

来源：

JOURNAL OF CHEMICAL SCIENCES | 2022年 / 134卷 / 03期

关键词：

Mesoporous; Diatomite; Xanthenes; Catalyst; Solvent-free; HETEROFUNCTIONAL CARRIER; COVALENT IMMOBILIZATION; ANTIBACTERIAL ACTIVITY; EFFICIENT SYNTHESIS; HIGHLY EFFICIENT; GREEN SYNTHESIS; SULFONIC-ACID; CONVENIENT; SULFONAMIDES; DERIVATIVES;

D O I：

10.1007/s12039-022-02065-x

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A new heterogeneous catalyst, nanodiatomite@melamine-SO3H, was introduced for synthesizing 1,8-dioxo-octahydroxanthenes via multicomponent reactions of aldehydes and dimedone. The prepared catalyst was characterized by employing several techniques, including FT-IR, XRD, TGA, EDX, BET, SEM, and TEM. The products were obtained under solvent-free conditions, with high yields in short reaction times. The nanodiatomite@melamine-SO3H was reused five times without substantial activity loss.

引用

页数：13

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