A Novel, Heterogeneous and Recyclable Polymeric Catalyst for the One-Pot Synthesis of Polyhydroquinoline and 1,8-Dioxohexahydroacridine Derivatives Under Solvent-Free Conditions

被引：0

作者：

Maleki, Behrooz ^{[1
]}

Tayebee, Reza ^{[1
]}

Sepehr, Zeinalabedin ^{[1
]}

Kermanian, Mina ^{[1
]}

机构：

[1] Hakim Sabzevari Univ, Dept Chem, Sabzevar 397, Iran

来源：

ACTA CHIMICA SLOVENICA | 2012年 / 59卷 / 04期

关键词：

Aldehydes; cyclic 1,3-dicarbonyl compounds; ammonium acetate; ethyl acetoacetate; crosslinked poly(AMPS-co-AA) catalyst; solvent-free; one-pot synthesis; SILICA SULFURIC-ACID; 4 COMPONENT CONDENSATION; EFFICIENT SYNTHESIS; HANTZSCH REACTION; BENZYLIC ALCOHOLS; REUSABLE CATALYST; HIGHLY EFFICIENT; AMMONIUM-NITRATE; SOLID ACID; ONE-STEP;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

An efficient, recyclable and environmental-friendly synthetic route to polyhdroquinoline and 1,8-dioxohexahydroacridine derivatives have been developed via multi-component one-pot Hantzsch reaction of various aldehydes and ammonium acetate with (a) cyclic 1,3-dicarbonyl compounds and ethyl acetoacetate, and (b) 2 equivalents of cyclic 1,3-dicarbonyl compounds in the presence of novel polymeric catalyst [poly(AMPS-co-AA)] under solvent-free conditions. The present approach offers several advantages such as short reaction times, easy isolation and purification of product, and safe, non-toxic, recyclable and economic use of catalyst.

引用

页码：814 / 823

页数：10

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