An efficient one-pot synthesis of 2-hydroxyalkyl dithiocarbamates

被引：24

作者：

Cui, JL ^{[1
]}

Ge, ZM ^{[1
]}

Cheng, TM ^{[1
]}

Li, RT ^{[1
]}

机构：

[1] Peking Univ, Sch Pharmaceut Sci, Dept Biol Chem, Beijing 100083, Haidian Dist, Peoples R China

来源：

SYNTHETIC COMMUNICATIONS | 2003年 / 33卷 / 12期

关键词：

2-hydroxyalkyl dithiocarbamate; ring opening of epoxide; regioselective reaction; anhydrous potassium phosphate; carbon disulfide;

D O I：

10.1081/SCC-120021023

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

In the presence of anhydrous potassium phosphate, epoxides reacted with carbon disulfide and primary or secondary amines in acetone to give the corresponding 2-hydroxyalkyl dithiocarbamates regioselectively in moderate to good yield.

引用

页码：1969 / 1976

页数：8

共 50 条

[31] Convenient, Efficient One-Pot Synthesis of Ferrocenylcyanide
Jun Long ZHANG
Chun E DONG
Yong Gang ZHI
Liang Fu ZHANG (Chengdu Institute of Organic Chemistry
ChineseChemicalLetters, 2000, (02) : 107 - 108
[32] An Efficient One-Pot Synthesis of Triamides and Amidodiesters
A. Shaabani
M. B. Teimouri
H. R. Bijanzadeh
Russian Journal of Organic Chemistry, 2004, 40 : 976 - 981
[33] Efficient one-pot synthesis of glycosyl disulfides
Morais, Goreti Ribeiro
Falconer, Robert A.
TETRAHEDRON LETTERS, 2007, 48 (43) : 7637 - 7641
[34] A new and efficient one-pot synthesis of indoles
Bratulescu, George
TETRAHEDRON LETTERS, 2008, 49 (06) : 984 - 986
[35] Highly Efficient Catalyst-Free One-Pot Synthesis of Dithiocarbamates under Solvent-Free Conditions
Guo, Shengrong
Yuan, Yanqin
Zhang, Chunniu
CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2012, 32 (05) : 907 - 914
[36] An efficient, basic resin-mediated, one-pot regioselective synthesis of 2-hydroxy alkyl dithiocarbamates from corresponding epoxides
Medicinal and Process Chemistry Division, Central Drug Research Institute, Lucknow-226001, U. P., India
不详
J. Sulfur Chem., 2007, 6 (607-612):
[37] A new and efficient one-pot procedure for the synthesis of 2-styrylquinolines
Dabiri, Minoo
Salehi, Peyman
Baghbanzadeh, Mostafa
Nikcheh, Maryam Shakouri
TETRAHEDRON LETTERS, 2008, 49 (37) : 5366 - 5368
[38] A simple and efficient one-pot synthesis of 2-substituted benzimidazoles
Bahrami, Kiumars
Khodaei, Mohammad Mehdi
Kavianinia, Iman
SYNTHESIS-STUTTGART, 2007, (04): : 547 - 550
[39] An efficient one-pot synthesis of 1,2,4-triazoloquinoxalines
Niu, Xiaoyi
Yang, Bingchuan
Fang, Shuai
Li, Yanqiu
Zhang, Zeyuan
Jia, Jiong
Ma, Chen
TETRAHEDRON, 2014, 70 (31) : 4657 - 4660
[40] Straightforward and highly efficient catalyst-free one-pot synthesis of dithiocarbamates under solvent-free conditions
Azizi, Najmedin
Aryanasab, Fezzeh
Saidi, Mohammad R.
ORGANIC LETTERS, 2006, 8 (23) : 5275 - 5277

← 1 2 3 4 5 →