A practical synthesis of novel hydroxyl-substituted macrocyclic tri-, tetra- and hexa-amines

被引：0

作者：

Xue, GP ^{[1
]}

Liu, Y ^{[1
]}

Wu, CT ^{[1
]}

机构：

[1] Wuhan Univ, Dept Chem, Wuhan 430072, Hubei, Peoples R China

来源：

CHINESE JOURNAL OF CHEMISTRY | 1998年 / 16卷 / 06期

关键词：

macrocyclic polyamine; cyclocondensation; mesocylic diamine;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Macrocyctic tri- and tetra-amines containing a hydroxyl group in the ring have been prepared in moderate yields by a. 1:1 cyclocondensation of 1,3-dichloro-2-propanol with the disodium salt of N-tosylated diethylenetriamine and triethylenetetraamine. In the case of condensation of 1,3-dichoro-2-propanol with the disodium salt of N-tosylated diethylenetriamine, the 2:2 cyclocondensation product, dihydroxyl macrocyclic hexaamine, was also isolated.

引用

页码：538 / 541

页数：4

共 50 条

[31] Preparation and properties of novel gramicidin S analogs possessing a tri-, tetra- or pentamethylene bridge between ornithine side chains
Yamada, K
Ando, K
Takahashi, Y
Oda, Y
Yamamura, H
Araki, S
Kobayashi, K
Katakai, R
Kato, F
Kawai, M
JOURNAL OF PEPTIDE RESEARCH, 1999, 53 (06): : 611 - 617
[32] Development and characterization of novel tetra-, tri- and di-nucleotide microsatellite markers in cacao (Theobroma cacao L.)
Ioná S. Araújo
Aline C. Intorne
Messias G. Pereira
Uilson V. Lopes
Gonçalo A. de Souza Filho
Molecular Breeding, 2007, 20 : 73 - 81
[33] Development and characterization of novel tetra-, tri- and di-nucleotide microsatellite markers in cacao (Theobroma cacao L.)
Araujo, Iona S.
Intorne, Aline C.
Pereira, Messias G.
Lopes, Uilson V.
de Souza Filho, Goncalo A.
MOLECULAR BREEDING, 2007, 20 (01) : 73 - 81
[34] Synthesis and structure of zirconium(IV) alkyl complexes with bi-, tri-, tetra- and penta-dentate amido ligands
Male, NAH
ThorntonPett, M
Bochmann, M
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1997, (14): : 2487 - 2494
[35] Current advances in the synthesis and biological potencies of tri- and tetra-substituted 1H-imidazoles
Majid M. Heravi
Mansoureh Daraie
Vahideh Zadsirjan
Molecular Diversity, 2015, 19 : 577 - 623
[36] Synthesis and Structural Analysis of Substituted Tripod-Shaped Tri- and Tetra(p-phenylene)s
Hierrezuelo, Jesus
Guillen, Elena
Manuel Lopez-Romero, J.
Rico, Rodrigo
Rosa Lopez-Ramirez, M.
Carlos Otero, J.
Cai, Chengzhi
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2010, 2010 (29) : 5672 - 5680
[37] Current advances in the synthesis and biological potencies of tri- and tetra-substituted 1H-imidazoles
Heravi, Majid M.
Daraie, Mansoureh
Zadsirjan, Vahideh
MOLECULAR DIVERSITY, 2015, 19 (03) : 577 - 623
[38] Hydromagnesiation of 1,3-Enynes by Magnesium Hydride for Synthesis of Tri- and Tetra-substituted Allenes
Wang, Bin
Li, Yihang
Pang, Jia Hao
Watanabe, Kohei
Takita, Ryo
Chiba, Shunsuke
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2021, 60 (01) : 217 - 221
[39] Straightforward synthesis of tri- and tetra-substituted 3-trifluoromethylfurans by heterocyclization reaction of perfluoroketene dithioacetals
De St Jores, Clement
Mukan, Ivan
Yegorova, Tatyana
Harakat, Dominique
Bouillon, Jean-Philippe
TETRAHEDRON, 2016, 72 (43) : 6807 - 6814
[40] A novel self-assembling of mixed tri- and dibutyltin macrocyclic complex with solvothermal synthesis method
Ma, Chunlin
Li, Qianli
Zhang, Rufen
INORGANICA CHIMICA ACTA, 2009, 362 (08) : 2937 - 2940

← 1 2 3 4 5 →