A practical synthesis of novel hydroxyl-substituted macrocyclic tri-, tetra- and hexa-amines

被引：0

作者：

Xue, GP ^{[1
]}

Liu, Y ^{[1
]}

Wu, CT ^{[1
]}

机构：

[1] Wuhan Univ, Dept Chem, Wuhan 430072, Hubei, Peoples R China

来源：

CHINESE JOURNAL OF CHEMISTRY | 1998年 / 16卷 / 06期

关键词：

macrocyclic polyamine; cyclocondensation; mesocylic diamine;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Macrocyctic tri- and tetra-amines containing a hydroxyl group in the ring have been prepared in moderate yields by a. 1:1 cyclocondensation of 1,3-dichloro-2-propanol with the disodium salt of N-tosylated diethylenetriamine and triethylenetetraamine. In the case of condensation of 1,3-dichoro-2-propanol with the disodium salt of N-tosylated diethylenetriamine, the 2:2 cyclocondensation product, dihydroxyl macrocyclic hexaamine, was also isolated.

引用

页码：538 / 541

页数：4

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