Microwave-assisted synthesis and characterization of novel metal-free and metallophthalocyanines containing four 13-membered dithiadiaza macrocycles

被引：23

作者：

Kantekin, Halit ^{[1
]}

Biyikliglu, Zekeriya ^{[1
]}

机构：

[1] Karadeniz Tech Univ, Dept Chem, Fac Arts & Sci, TR-61080 Trabzon, Turkey

来源：

DYES AND PIGMENTS | 2008年 / 77卷 / 01期

关键词：

phthalocyanine; dithiadiazamacrocycle; phthalonitrile; macrocyclization; tosylation;

D O I：

10.1016/j.dyepig.2007.03.012

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

Novel, tetrasubstituted metal-free phthalocyanine and metallophtalocyanines bearing four 13-membered dithiadiaza. macrocycle peripheral groups were synthesized by cyclotetramerization of the phthalonitrile derivative in a multi-step reaction sequence, The new compounds were characterized by a combination of IR, H-1 NMR, C-13 NMR, UV-vis, elemental analysis and MS spectral data. (C) 2007 Elsevier Ltd. All rights reserved.

引用

页码：98 / 102

页数：5

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