Microwave-assisted synthesis and characterization of novel metal-free and metallophthalocyanines containing four 13-membered dithiadiaza macrocycles

被引：23

作者：

Kantekin, Halit ^{[1
]}

Biyikliglu, Zekeriya ^{[1
]}

机构：

[1] Karadeniz Tech Univ, Dept Chem, Fac Arts & Sci, TR-61080 Trabzon, Turkey

来源：

DYES AND PIGMENTS | 2008年 / 77卷 / 01期

关键词：

phthalocyanine; dithiadiazamacrocycle; phthalonitrile; macrocyclization; tosylation;

D O I：

10.1016/j.dyepig.2007.03.012

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

Novel, tetrasubstituted metal-free phthalocyanine and metallophtalocyanines bearing four 13-membered dithiadiaza. macrocycle peripheral groups were synthesized by cyclotetramerization of the phthalonitrile derivative in a multi-step reaction sequence, The new compounds were characterized by a combination of IR, H-1 NMR, C-13 NMR, UV-vis, elemental analysis and MS spectral data. (C) 2007 Elsevier Ltd. All rights reserved.

引用

页码：98 / 102

页数：5

共 50 条

[1] The microwave-assisted synthesis and characterization of novel metal-free and metallophthalocyanines peripherally fused to four 13-membered diazadithia macrocycles
Celenk, Elif
Kantekin, Halit
[J]. DYES AND PIGMENTS, 2009, 80 (01) : 93 - 97
[2] Microwave-assisted synthesis and characterization of novel metal-free and metallophthalocyanines containing four 14-membered tetraaza macrocycles
Biyiklioglu, Zekeriya
Kantekin, Halit
Oezil, Musa
[J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2007, 692 (12) : 2436 - 2440
[3] A novel metal-free and metallophthalocyanines containing four 19-membered dithiadiazadioxa macrocycles by microwave irradiation: Synthesis and characterization
Biyikhoglu, Zekeriya
Kantekin, Halit
[J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2008, 693 (03) : 505 - 509
[4] Microwave-assisted synthesis and characterization of a new soluble metal-free and metallophthalocyanines peripherally fused to four 18-membered tetrathiadiaza macrocycles
Kantekin, Halit
Dilber, Guelsev
Nas, Asiye
[J]. JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2010, 695 (08) : 1210 - 1214
[5] Microwave assisted synthesis and characterization of novel metal-free and metallophthalocyanines containing four pyridyl groups
Zekeriya Bıyıklıoğlu
Halit Kantekin
[J]. Transition Metal Chemistry, 2007, 32 : 851 - 856
[6] Microwave assisted synthesis and characterization of novel metal-free and metallophthalocyanines containing four pyridyl groups
Biyiklioglu, Zekeriya
Kantekin, Halit
[J]. TRANSITION METAL CHEMISTRY, 2007, 32 (07) : 851 - 856
[7] Microwave-assisted synthesis and characterization of a new metal-free and metallophthalocyanines
Kilicaslan, Meltem B.
Agin, Fatma
Kantekin, Halit
[J]. JOURNAL OF COORDINATION CHEMISTRY, 2010, 63 (05) : 861 - 867
[8] The synthesis and characterization of new metal-free and metallophthalocyanines containing four 27-membered diazaheptathia macrocycles
Gok, H. Zeki
Kantekin, Halit
Gok, Yasar
Herman, Gerrit
[J]. DYES AND PIGMENTS, 2007, 75 (03) : 606 - 611
[9] The synthesis and characterization of novel metal-free and metallophthalocyanines bearing four 27-membered dioxadiazapentathia macrocycles
Gok, H. Zeki
Kantekin, Halit
Gok, Yasar
Herman, Gerrit
[J]. DYES AND PIGMENTS, 2007, 74 (03) : 699 - 705
[10] Synthesis and characterization of metal-free and metallophthalocyanines containing four 17-membered dioxa-triaza macrocycles
Yildiz, SZ
Gök, Y
[J]. NEW JOURNAL OF CHEMISTRY, 1998, 22 (12) : 1365 - 1369

← 1 2 3 4 5 →