Deposition of iron sulfide thin films by AACVD from single source precursors

被引：34
|
作者：
Akhtar, Masood
Abdelhady, Ahmed Lutfi
Malik, M. Azad
O'Brien, Paul [1 ]
机构：
[1] Univ Manchester, Sch Chem, Manchester M13 9PL, Lancs, England
来源：
JOURNAL OF CRYSTAL GROWTH | 2012年 / 346卷 / 01期
基金：
英国工程与自然科学研究理事会;
关键词：
Crystallites; Substrates; Aerosol assisted chemical vapor deposition (AACVD); Cubic pyrite; Hexagonal pyrrhotite; tris(dialkyldithiocarbamato)iron(III); FES2; PYRITE; NANOPARTICLES; GROWTH; PYRRHOTITE; CHEMISTRY; COMPLEX;
D O I：
10.1016/j.jcrysgro.2012.02.013
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The unsymmetrical [Fe((S2CNEtPr)-Pr-i)(3)] (1), [Fe(S2CNEtMe)(3)] (2) and symmetrical [Fe(S2CN(Hex)(2))(3)] (3), Fe(S2CN(Et)(2))(3)] (4) tris(dialkyldithiocarbamato)iron(III) complexes were used as single source precursors for the deposition of iron sulfide thin films by the aerosol assisted chemical vapor Deposition (AACVD) method. The unsymmetrical complexes deposited the mixed phases (pyrite and marcasite) at all deposition temperatures except the complex (2) which deposited pyrite and pyrrhotite at 400 degrees C. The symmetrical complex (3) with longer alkyl groups produced a mixture of pyrite and pyrrhotite phases at 350 and 450 degrees C but pyrite and mackinawite at 400 degrees C whereas the complex (4) with shorter alkyl groups deposited a mixture of pyrite and marcasite at 350 degrees C but a pure pyrrhotite phase at 400 and 450 degrees C. (C) 2012 Elsevier B.V. All rights reserved.
引用
收藏
页码：106 / 112
页数：7
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