1,1′,5,5′-Tetramethyl-2,2′-diphenyl-4,4′-[p-phenylenebis(methylidynenitrilo)]di-1H-pyrazol-3(2H)-one

被引:0
|
作者
Xiao, Yan [1 ]
Bi, Cai Feng [1 ]
Wang, Ai Dong [1 ]
Fan, Yu Hua [1 ]
Zhang, Xia [1 ]
Xu, Jia Kun [1 ]
Xie, Si Tang [1 ]
机构
[1] Ocean Univ China, Coll Chem, Minist Educ, Key Lab Marine Chem Theory & Technol, Qingdao 266100, Shandong, Peoples R China
关键词
D O I
10.1107/S1600536808021028
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the centrosymmetric title compound, C30H28N6O2, the dihedral angles between the antipyrine ring and the terminal phenyl and central benzene rings are 50.55 (10) and 14.62(9)degrees, respectively. Some short intermolecular C-H center dot center dot center dot O interactions may help to establish the packing. An intramolecular C-H center dot center dot center dot O hydrogen bond is also present.
引用
收藏
页码:O1479 / U2174
页数:9
相关论文
共 50 条
  • [31] REACTION OF 5,5,5',5'-TETRAMETHYL-2,2'-AZO-1,1'-PYRROLINE 1,1'-DIOXIDE WITH SULPHINIC ACIDS
    FORRESTE.AR
    THOMSON, RH
    JOURNAL OF THE CHEMICAL SOCIETY C-ORGANIC, 1966, (04): : 382 - &
  • [32] meso-2,2′-Diphenyl-3,3′,4,4′-tetrahydro-2,2′-bifuran-5,5′(2H,2′H)-dione
    Billing, DG
    Holzapfel, CW
    Blann, K
    Williams, DBG
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2000, 56 (11): : E522 - E523
  • [33] 4-[(5-Hydroxy-3-methyl-1-phenyl-1H-pyrazol-4-yl)phenylmethyl]-5-methyl-2-phenyl-1H-pyrazol-3(2H)-one ethanol hemisolvate
    Fun, Hoong-Kun
    Kia, Reza
    Girish, K. S.
    Kalluraya, B.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O66 - U1836
  • [34] 4-[(4-Chlorophenyl)(5-hydroxy-3-methyl-1-phenyl-1H-pyrazol-4-yl) methyl]-5-methyl-2-phenyl-1H-pyrazol-3(2H)-one
    Fun, Hoong-Kun
    Jebas, Samuel Robinson
    Girish, K. S.
    Kalluraya, B.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O2301 - U1984
  • [35] 2-(4-Chlorophenyl)-4-[1-(4-chlorophenyl)-3-methyl-1H-pyrazol-5-yl]-5-methyl-1H-pyrazol-3(2H)-one
    Rabnawaz, Muhammad
    Shah, Muhammad Raza
    Ng, Seik Weng
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2569 - U535
  • [36] A novel class of naturally occurring halogenated pyrroles, 1,1′-dimethyl-3,3′,4,4′,5,5′-hexabromo-2,2′-bipyrrole, 5,5′-dichloro-1,1′-dimethyl-3,3′,4,4′-tetrabromo-2,2′-bipyrrole, and 1,1′-dimethyl-3,3′,4,4′,5,5′-hexachloro-2,2′-bipyrrole
    Blank, DH
    Gribble, GW
    Schneekloth, JS
    Jasinski, JP
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2002, 32 (12) : 541 - 546
  • [37] A novel class of naturally occurring halogenated pyrroles, 1,1′-dimethyl-3,3′,4,4′,5,5′-hexabromo-2,2′-bipyrrole, 5,5′-dichloro-1,1′-dimethyl-3,3′,4,4′-tetrabromo-2,2′-bipyrrole, and 1,1′-dimethyl-3,3′,4,4′,5,5′-hexachloro-2,2′-bipyrrole
    David H. Blank
    Gordon W. Gribble
    John S. Schneekloth
    Jerry P. Jasinski
    Journal of Chemical Crystallography, 2002, 32 : 541 - 546
  • [38] 4-[(5-Chloro-3-methyl-1-phenyl-1H-pyrazol-4-yl)methylideneamino]-1,5dimethyl-2-phenyl-1H-pyrazol-3(2H)one
    Zhu, Hualing
    Zhu, Jinhua
    Ban, Litong
    Zhang, Pingping
    Zhang, Miao
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2724 - U1784
  • [39] Synthesis and dynamic solution behavior of 2,2′,5,5′-tetrakis (trimethylsilyl)-3,3′,4,4′-tetramethyl-1,1′-diphosphaferrocene
    Al-Taweel, SM
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1997, 130 : 203 - 209
  • [40] 1,1′,2,2′-Tetramethyl-3,3′-(4-methoxybenzylidene)di-1H-indole
    Zhang, Cai-Li
    Ye, Ping-Ping
    Du, Zhi-Qiang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O1332 - U2323