Synthesis of 4-(N,N-Dialkylamino) benzyltriphenylphosphonium Iodides from Hydroxymethyltriphenylphosphonium Iodide and N,N-Dialkylaniline

被引：5

作者：

Davis, Matthew C. ^{[1
]}

Parrish, Damon A. ^{[2
]}

机构：

[1] USN, Air Warfare Ctr, Michelson Lab, Chem & Mat Div, China Lake, CA 93555 USA

[2] USN, Res Lab, Struct Matter Lab, Washington, DC 20375 USA

来源：

SYNTHETIC COMMUNICATIONS | 2008年 / 38卷 / 22期

关键词：

Formaldehyde; N; N-dialkylaniline; triphenylphosphine; Wittig;

D O I：

10.1080/00397910802238783

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Reinvestigation of the one-pot synthesis of 4-(N,N-dialkylamino)benzyltriphenylphosphonium iodides has shown that the product forms after the initial condensation of triphenylphosphine upon formaldehyde.

引用

页码：3909 / 3918

页数：10

共 50 条

[41] Solid phase synthesis of N,N-dialkylaniline derivatives on ACT high-pressure reaction blocks, ARES REACTORS.
Saavedra, OM
Fernandez-Saiz, M
Saneii, H
Lou, BL
ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2001, 221 : U116 - U117
[42] STUDIES OF N-OXIDES OF N,N-DIALKYLAMINO ACIDS .4. DECARBOXYLATION OF N,N-DIMETHYLAMINO ACID N-OXIDES WITH PARA TOLUENESULFONYL CHLORIDE IN PYRIDINE
IKUTANI, Y
BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1971, 44 (01) : 271 - +
[43] PREPARATION OF PHENYLGLYCOLIC ACIDS AND SODIUM P-(N,N-DIALKYLAMINO)PHENYLGLYCOLATES
KATRITZKY, AR
GALUSZKA, B
RACHWAL, S
LYNCH, D
ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 1993, 25 (05) : 557 - 562
[44] STUDIES OF N-OXIDES OF N,N-DIALKYLAMINO ACIDS .2. SYNTHESES OF N,N-DIALKYLGLYCINE AND CORRESPONDING N-OXIDES
IKUTANI, Y
BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1969, 42 (08) : 2330 - +
[45] Unexpected dealkylation during nucleophilic substitution:: Synthesis of 2-N,N-dialkylamino benzoxazoles and benzothiazoles
Khalaf, AI
Alvarez, RG
Suckling, CJ
Waigh, RD
TETRAHEDRON, 2000, 56 (43) : 8567 - 8571
[46] BIS-(N,N-DIALKYLAMINO)-ALKOXYPHOSPHINES AS A NEW CLASS OF PHOSPHITE COUPLING AGENT FOR THE SYNTHESIS OF OLIGONUCLEOTIDES
LEE, HJ
MOON, SH
CHEMISTRY LETTERS, 1984, (07) : 1229 - 1232
[47] SYNTHESIS OF N,N,N-TRIETHYL-2-[4-(2-PHENYLETHENYL)PHENOXY] ETHANAMMONIUM IODIDE
ALHASSAN, MI
SYNTHETIC COMMUNICATIONS, 1989, 19 (9-10) : 1677 - 1680
[48] Remarkable diastereoselectivity in the addition of allylic and unsaturated diorganozinc reagents to β-(N,N-dialkylamino)-aldehydes
Soucy, RL
Kozhinov, D
Behar, V
JOURNAL OF ORGANIC CHEMISTRY, 2002, 67 (06): : 1947 - 1952
[49] Simple and Mild Syntheses of Optically Active 2-(N,N-Dialkylamino)oxazolines
JIA Xu-dong
Chemical Research in Chinese Universities, 2010, 26 (03) : 394 - 397
[50] Simple and Mild Syntheses of Optically Active 2-(N,N-Dialkylamino)oxazolines
Jia Xu-dong
Duan Hai-feng
Lin Ying-jie
Cao Jun-gang
Liang Da-peng
Luo Xu-yang
Jiang Feng
Gao Han
Wu Mao-cheng
CHEMICAL RESEARCH IN CHINESE UNIVERSITIES, 2010, 26 (03) : 394 - 397

← 1 2 3 4 5 →