Synthesis of 4-(N,N-Dialkylamino) benzyltriphenylphosphonium Iodides from Hydroxymethyltriphenylphosphonium Iodide and N,N-Dialkylaniline

被引：5
|
作者：
Davis, Matthew C. [1 ]
Parrish, Damon A. [2 ]
机构：
[1] USN, Air Warfare Ctr, Michelson Lab, Chem & Mat Div, China Lake, CA 93555 USA
[2] USN, Res Lab, Struct Matter Lab, Washington, DC 20375 USA
来源：
SYNTHETIC COMMUNICATIONS | 2008年 / 38卷 / 22期
关键词：
Formaldehyde; N; N-dialkylaniline; triphenylphosphine; Wittig;
D O I：
10.1080/00397910802238783
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Reinvestigation of the one-pot synthesis of 4-(N,N-dialkylamino)benzyltriphenylphosphonium iodides has shown that the product forms after the initial condensation of triphenylphosphine upon formaldehyde.
引用
收藏
页码：3909 / 3918
页数：10
相关论文
共 50 条
  • [31] THE SYNTHESIS AND PROPERTIES OF SOME SUBSTITUTED PHENYL OMEGA-(N,N-DIALKYLAMINO)-ALKYL SULFIDES
    SCHUETZ, RD
    BALDWIN, RA
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1958, 80 (01) : 162 - 164
  • [32] The Analogy Between C-O and C=C(CN)2: Structural Properties of 3-(N,N-Dialkylamino)propenones and 4-(N,N-Dialkylamino)-1,1- dicyano-1,3-butadienes
    Acta Chem Scand, 4 (391):
  • [33] Synthesis of 2,5-bis(N,N-dialkylamino)thiophenes or 1-alkyl-2-N,N-dialkylamino-5-methylthiopyrroles from propargylic amines and isothiocyanates
    Tarasova, OA
    Nedolya, NA
    Vvedensky, VY
    Brandsma, L
    Trofimov, BA
    TETRAHEDRON LETTERS, 1997, 38 (41) : 7241 - 7242
  • [34] REACTIVITY OF THE RADICAL-CATION OF 4-(N,N-DIALKYLAMINO)BIPHENYL DERIVATIVES AS PROBED BY RESONANCE RAMAN-SPECTROSCOPY
    BENBOUAZZA, A
    BUNTINX, G
    POIZAT, O
    SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 1993, 49 (10): : 1487 - 1494
  • [35] Anodic voltammetry of C-(N,N-dialkylamino)-substituted phosphaalkenes
    Zagumennov, V. A.
    RUSSIAN JOURNAL OF ELECTROCHEMISTRY, 2011, 47 (11) : 1317 - 1318
  • [36] THE REACTION OF C-(N,N-DIALKYLAMINO)PHOSPHAALKENES AND THEIR DIMERS WITH SULFUR
    IONKIN, AS
    IGNATEVA, SN
    ARBUZOV, BA
    BULLETIN OF THE ACADEMY OF SCIENCES OF THE USSR DIVISION OF CHEMICAL SCIENCE, 1990, 39 (05): : 1052 - 1054
  • [37] SYNTHESIS AND CHARACTERIZATION OF SOME BORANE DERIVATIVES OF DIALKYL-1-(N,N-DIALKYLAMINO)ALKYLPHOSPHONATES
    KAUSHIK, MP
    CHARANDABI, RMD
    LOFTHOUSE, TJ
    ETTEL, ML
    MORSE, KW
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1988, 196 : 233 - INOR
  • [38] Synthesis of 2,5-bis(N,N-dialkylamino)thiophenes or 1-alkyl-2-N,N-dialkylamino-5-methylthiop yrroles from propargylic amines and isothiocyanates
    Tetrahedron Lett, 41 (7241):
  • [39] Synthesis and characterization of the poly(sulfobetaine)s and the corresponding cationic polymers derived from N,N-dialkylamino phenyl methacrylamide
    Liaw, DJ
    Huang, CC
    MACROMOLECULAR CHEMISTRY AND PHYSICS, 2000, 201 (11) : 1101 - 1107
  • [40] Gas chromatography/mass spectrometry analysis of reaction products of Chemical Weapons Convention-related 2-(N,N-dialkylamino)ethylchlorides with 2-(N,N-dialkylamino)ethanols
    Rodda, Ramesh
    Malkapuri, Nikita Singh
    Addipilli, Ramunaidu
    Vattem Venkata, Swarajya Lakshmi
    Kantevari, Srinivas
    Thota, Jagadeshwar Reddy
    Sripadi, Prabhakar
    RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 2024, 38 (16)
12345