Electrodeposition of Nanocrystalline Ni-W Coatings with Citric Acid System

被引:12
|
作者
Du, Jingjing [1 ,2 ]
Xu, Lijian [1 ,2 ]
Chen, Baizhen [1 ]
Li, De [3 ]
机构
[1] Cent S Univ, Sch Met Sci & Engn, Changsha 410083, Hunan, Peoples R China
[2] Hunan Univ Technol, Hunan Key Lab Green Packaging & Applicat Biol Nan, Zhuzhou 412008, Peoples R China
[3] Hunan Changgao High Voltage Switchgear Grp Co Ltd, Changsha 410219, Hunan, Peoples R China
基金
中国国家自然科学基金;
关键词
Ni-W Alloy Coatings; Citric Acid; Nanocrystalline; Electrodeposition; ELECTROCHROMIC PROPERTIES; NANOPARTICLES; RESISTANCE;
D O I
10.1166/jnn.2013.6850
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Ni-W alloy coatings were prepared by electrodeposition technique with citric acid as a complexing agent. The influence of the main technical parameters on W content in the Ni-W alloy coatings were investigated by electron dispersive spectroscopy (EDS), and the microstructure of the coatings was characterized and analyzed by employing X-ray diffractometer (XRD), scanning electron microscope (SEM). The results showed that bright and compact Ni-W alloy coatings with 25.78 wt% W were obtained when the concentration of Na2WO4 center dot 2H(2)O was 50 g/L, the concentration of NH4Cl was 20 g/L, the bath pH value was 8.0 and the bath temperature was 70 degrees C. The surface of Ni-W alloy coatings were bright, flat and compact, the mircostructure of the alloy coatings were nanocrystalline and the average grain size was about 38 nm by calculating using Scherrer Equation.
引用
收藏
页码:690 / 693
页数:4
相关论文
共 50 条
  • [21] Pulse current electrodeposition and corrosion properties of Ni-W alloy coatings
    Zemanova, M.
    Krivosudska, M.
    Chovancova, M.
    Jorik, V.
    [J]. JOURNAL OF APPLIED ELECTROCHEMISTRY, 2011, 41 (09) : 1077 - 1085
  • [22] Co-electrodeposition of hard Ni-W/diamond nanocomposite coatings
    Zhang, Xinyu
    Qin, Jiaqian
    Das, Malay Kumar
    Hao, Ruru
    Zhong, Hua
    Thueploy, Adisak
    Limpanart, Sarintorn
    Boonyongmaneerat, Yuttanant
    Ma, Mingzhen
    Liu, Riping
    [J]. SCIENTIFIC REPORTS, 2016, 6
  • [23] Electrodeposition and characterization of Ni-W/ZrO2 nanocomposite coatings
    Zhao, Chunmei
    Yao, Yingwu
    He, Liang
    [J]. BULLETIN OF MATERIALS SCIENCE, 2014, 37 (05) : 1053 - 1058
  • [24] Electrodeposition and characterization of Ni-W/ZrO2 nanocomposite coatings
    Chunmei Zhao
    Yingwu Yao
    Liang He
    [J]. Bulletin of Materials Science, 2014, 37 : 1053 - 1058
  • [25] Effect of β-cyclodextrin as Organic Additive on Pulse Electrodeposition of Nanocrystalline Ni-W Coating
    Yang, Qiangbin
    He, Yi
    Fan, Yi
    Zhan, Yingqing
    Tang, Ying
    [J]. INTERNATIONAL JOURNAL OF ELECTROCHEMICAL SCIENCE, 2016, 11 (06): : 5103 - 5110
  • [26] Electrodeposition and mechanical and corrosion resistance properties of Ni-W/SiC nanocomposite coatings
    Yao, Yingwu
    Yao, Suwei
    Zhang, Lu
    Wang, Hongzhi
    [J]. MATERIALS LETTERS, 2007, 61 (01) : 67 - 70
  • [27] Development of Electrodeposition Bath Using a Substitute of Propionic Acid for Bulk Nanocrystalline Ni-W Alloys with High Ductility
    Matsui, Isao
    Omura, Naoki
    Li, Mingjun
    Murakami, Yuichiro
    Tada, Shuji
    [J]. JOURNAL OF THE JAPAN INSTITUTE OF METALS AND MATERIALS, 2016, 80 (03) : 217 - 223
  • [28] Corrosion and tribological properties of nanocrystalline pulse electrodeposited Ni-W alloy coatings
    Druga, J.
    Kasiarova, M.
    Dobrocka, E.
    Zemanova, M.
    [J]. TRANSACTIONS OF THE INSTITUTE OF METAL FINISHING, 2017, 95 (01): : 39 - 45
  • [29] Deposition and characterization of nanocrystalline and amorphous Ni-W coatings with embedded alumina nanoparticles
    Yari, Saeed
    Dehghanian, Changiz
    [J]. CERAMICS INTERNATIONAL, 2013, 39 (07) : 7759 - 7766
  • [30] Influence of compositional and microstructural gradient on the wear performance of nanocrystalline Ni-W coatings
    Lavakumar, B.
    Prasad, M. J. N. V.
    Phani, P. Sudharshan
    Wasekar, Nitin P.
    [J]. WEAR, 2023, 530