Influence of pH on physical properties of nickel-zinc nanocrystalline powders synthesized by a sol-gel auto-combustion method

被引：3
|
作者：
Barati, M. R. [1 ]
Ebrahimi, S. A. Seyyed [1 ]
Badiei, A. [2 ]
机构：
[1] Univ Tehran, Sch Met & Mat Eng, Ctr Excellence Magnet Mat, Tehran, Iran
[2] Univ Tehran, Sch Chem, Tehran, Iran
来源：
INTERNATIONAL JOURNAL OF MODERN PHYSICS B | 2008年 / 22卷 / 18-19期
关键词：
nickel-zinc; nanocrystalline; sol-gel; auto combustion;
D O I：
10.1142/S0217979208048048
中图分类号：
O59 [应用物理学];
学科分类号：
摘要：
In this research a sol-gel auto-combustion route has been proposed to synthesize nickel-zinc ferrite nanocrystalline powder, using metal nitrates, citric acid as fuel and ammonia as pH adjusting agent. The influence of pH value of the solution on phase evolution, crystallite size and morphology of as-burnt powders were investigated by XRD, SEM and TEM techniques. The results revealed that with pH=7 the single phase nickel-zinc ferrite nanocrystalline powders with crystallite size of about 27nm were formed directly after auto combustion process.
引用
收藏
页码：3153 / 3158
页数：6
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