Synthesis and characterization of nanocrystalline spinel Zinc ferrite prepared by sol-gel auto-combustion technique

被引:20
|
作者
Khorrami, S. [1 ]
Gharib, F. [2 ]
Mahmoudzadeh, G. [1 ]
Sepehr, S. Sadat [1 ]
Madani, S. Sadat [1 ]
Naderfar, N. [1 ]
Manie, S. [1 ]
机构
[1] Islamic Azad Univ, Dept Chem, North Tehran Branch, Tehran, Iran
[2] Shahid Beheshti Univ, Dept Chem, Tehran, Iran
关键词
Sol-gel auto-combustion; Nanocrystalline; ZnFe2O4; X-ray diffraction; Scanning electron microscopy;
D O I
10.7508/ijnd.2010.03.005
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Sol-gel auto-combustion is a unique combination of the combustion and the chemical gelation processes. In this work, nanosize (d) powders with compositions of ZnFe2O4 were synthesized by sol-gel combustion method. The puffy, porous brown powders as-combusted was calcined at the temperature of 750-1000 degrees C for 4 h. These powders are characterized by X-ray diffraction and scanning electron microscopy. Particle size and morphology of nanocrystalline were determined by XRD and SEM, respectively. The average particle size was estimated about 17 nm for calcined powders. Surface area for zinc ferrite synthesized by this method is 36 m(2)/g.
引用
收藏
页码:221 / 224
页数:4
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