A convenient and efficient one-pot synthesis of 3-acylisoxazoles using iron(III) salts

被引:25
|
作者
Itoh, K
Sakamaki, H
Nakazato, N
Horiuchi, A
Horn, E
Horiuchi, CA
机构
[1] Rikkyo St Pauls Univ, Dept Chem, Toshima Ku, Tokyo 1718501, Japan
[2] Nihon Univ, Coll Sci & Technol, Funabashi, Chiba 2748501, Japan
来源
SYNTHESIS-STUTTGART | 2005年 / 20期
关键词
alkenes; alkynes; ketones; iron(III) nitrate; 3-acylisoxazoles;
D O I
10.1055/s-2005-916041
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
3-Acylisoxazoles were synthesized by the reaction of alkenes or alkynes with ketones (acetone or acetophenone), as both a reagent and the solvent, by three methods: iron(III) nitrate under reflux, iron(III) salt-nitrogen dioxide (NO2) at room temperature, and iron(III) nitrate under microwave irradiation (MW).
引用
收藏
页码:3541 / 3548
页数:8
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