A convenient one-pot synthesis of 1,2-azaphospholanium salts

被引：10
|
作者：
Aladzheva, IM [1 ]
Lobanov, DI [1 ]
Bykhovskaya, OV [1 ]
Petrovskii, PV [1 ]
Lyssenko, KA [1 ]
Mastryukova, TA [1 ]
机构：
[1] Russian Acad Sci, AN Nesmeyanov Organoelement Cpds Inst, Moscow 119991, Russia
来源：
HETEROATOM CHEMISTRY | 2003年 / 14卷 / 07期
关键词：
D O I：
10.1002/hc.10209
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A novel facile one-pot synthesis of the 1,2-azaphospholanes by intramolecular alkylation of 3-halopropyl amides of tricoordinate phosphorus has been suggested. Using this method, a series of the differently N-substituted 1,2-azaphospholanium salts were synthesized. 3-Aminopropylphosphine oxides were obtained by hydrolysis of the salts. A probable mechanism of the 1,2-azaphospholanium salts formation is discussed. (C) 2003 Wiley Periodicals, Inc.
引用
收藏
页码：596 / 602
页数：7
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