Development of multi-frequency ESR system for high-pressure measurements up to 2.5 GPa

被引：32
|
作者：
Sakurai, T. [1 ]
Fujimoto, K. [2 ]
Matsui, R. [2 ]
Kawasaki, K. [2 ]
Okubo, S. [3 ]
Ohta, H. [2 ,3 ]
Matsubayashi, K. [4 ]
Uwatoko, Y. [4 ]
Tanaka, H. [5 ]
机构：
[1] Kobe Univ, Ctr Supports Res & Educ Act, Nada Ku, Kobe, Hyogo 6578501, Japan
[2] Kobe Univ, Grad Sch Sci, Nada Ku, Kobe, Hyogo 6578501, Japan
[3] Kobe Univ, Mol Photosci Res Ctr, Nada Ku, Kobe, Hyogo 6578501, Japan
[4] Univ Tokyo, Inst Solid State Phys, Kashiwa, Chiba 2778581, Japan
[5] Tokyo Inst Technol, Dept Phys, Meguro Ku, Tokyo 1528550, Japan
来源：
JOURNAL OF MAGNETIC RESONANCE | 2015年 / 259卷
基金：
日本学术振兴会;
关键词：
High-pressure ESR; Hybrid-type pressure cell; ZrO2-based ceramic; NiSnCl6 center dot 6H(2)O; CsCuCl3; HIGH-FIELD; CELL;
D O I：
10.1016/j.jmr.2015.08.005
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A new piston-cylinder pressure cell for electron spin resonance (ESR) has been developed. The pressure cell consists of a double-layer hybrid-type cylinder with internal components made of the ZrO2-based ceramics. It can generate a pressure of 2 GPa repeatedly and reaches a maximum pressure of around 2.5 GPa. A high-pressure ESR system using a cryogen-free superconducting magnet up 10T has also been developed for this hybrid-type pressure cell. The frequency region is from 50 GHz to 400 GHz. This is the first time a pressure above 2 GPa has been achieved in multi-frequency ESR system using a piston-cylinder pressure cell. We demonstrate its potential by showing the results of the high-pressure ESR of the S = 1 system with the single ion anisotropy NiSnCl6 center dot 6H(2)O and the S = 1/2 quantum spin system CsCuCl3. We performed ESR measurements of these systems above 2 GPa successfully. (C) 2015 Elsevier Inc. All rights reserved.
引用
收藏
页码：108 / 113
页数：6
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