Development of multi-frequency ESR system for high-pressure measurements up to 2.5 GPa

被引：32
|
作者：
Sakurai, T. [1 ]
Fujimoto, K. [2 ]
Matsui, R. [2 ]
Kawasaki, K. [2 ]
Okubo, S. [3 ]
Ohta, H. [2 ,3 ]
Matsubayashi, K. [4 ]
Uwatoko, Y. [4 ]
Tanaka, H. [5 ]
机构：
[1] Kobe Univ, Ctr Supports Res & Educ Act, Nada Ku, Kobe, Hyogo 6578501, Japan
[2] Kobe Univ, Grad Sch Sci, Nada Ku, Kobe, Hyogo 6578501, Japan
[3] Kobe Univ, Mol Photosci Res Ctr, Nada Ku, Kobe, Hyogo 6578501, Japan
[4] Univ Tokyo, Inst Solid State Phys, Kashiwa, Chiba 2778581, Japan
[5] Tokyo Inst Technol, Dept Phys, Meguro Ku, Tokyo 1528550, Japan
来源：
JOURNAL OF MAGNETIC RESONANCE | 2015年 / 259卷
基金：
日本学术振兴会;
关键词：
High-pressure ESR; Hybrid-type pressure cell; ZrO2-based ceramic; NiSnCl6 center dot 6H(2)O; CsCuCl3; HIGH-FIELD; CELL;
D O I：
10.1016/j.jmr.2015.08.005
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A new piston-cylinder pressure cell for electron spin resonance (ESR) has been developed. The pressure cell consists of a double-layer hybrid-type cylinder with internal components made of the ZrO2-based ceramics. It can generate a pressure of 2 GPa repeatedly and reaches a maximum pressure of around 2.5 GPa. A high-pressure ESR system using a cryogen-free superconducting magnet up 10T has also been developed for this hybrid-type pressure cell. The frequency region is from 50 GHz to 400 GHz. This is the first time a pressure above 2 GPa has been achieved in multi-frequency ESR system using a piston-cylinder pressure cell. We demonstrate its potential by showing the results of the high-pressure ESR of the S = 1 system with the single ion anisotropy NiSnCl6 center dot 6H(2)O and the S = 1/2 quantum spin system CsCuCl3. We performed ESR measurements of these systems above 2 GPa successfully. (C) 2015 Elsevier Inc. All rights reserved.
引用
收藏
页码：108 / 113
页数：6
相关论文
共 50 条
  • [1] Development of High-Pressure and Multi-Frequency ESR System and Its Application to Quantum Spin System
    Sakurai, Takahiro
    Matsui, Ryosuke
    Kawasaki, Kohei
    Okubo, Susumu
    Ohta, Hitoshi
    Matsubayashi, Kazuyuki
    Uwatoko, Yoshiya
    Kudo, Kazutaka
    Koike, Yoji
    APPLIED MAGNETIC RESONANCE, 2015, 46 (09) : 1007 - 1012
  • [2] Development of High-Pressure and Multi-Frequency ESR System and Its Application to Quantum Spin System
    Takahiro Sakurai
    Ryosuke Matsui
    Kohei Kawasaki
    Susumu Okubo
    Hitoshi Ohta
    Kazuyuki Matsubayashi
    Yoshiya Uwatoko
    Kazutaka Kudo
    Yoji Koike
    Applied Magnetic Resonance, 2015, 46 : 1007 - 1012
  • [3] Development of a multi-frequency ESR system with high sensitivity
    Yashiro, H.
    Kashiwagi, T.
    Horitani, M.
    Hobo, F.
    Hori, H.
    Hagiwara, M.
    YAMADA CONFERENCE LX ON RESEARCH IN HIGH MAGNETIC FIELDS, 2006, 51 : 576 - +
  • [4] Development of high-pressure, high-field and multi-frequency ESR apparatus and its application to quantum spin system
    Sakurai, T.
    Horie, T.
    Tomoo, M.
    Kondo, K.
    Matsumi, N.
    Okubo, S.
    Ohta, H.
    Uwatoko, Y.
    Kudo, K.
    Koike, Y.
    Tanaka, H.
    INTERNATIONAL CONFERENCE ON HIGH PRESSURE SCIENCE AND TECHNOLOGY, JOINT AIRAPT-22 AND HPCJ-50, 2010, 215
  • [5] Development of Pressure Calibration Method in High-Pressure THz ESR System
    Takahiro Sakurai
    Yoshimasa Yasutani
    Hitoshi Sugawara
    Susumu Okubo
    Hitoshi Ohta
    Applied Magnetic Resonance, 2022, 53 : 763 - 775
  • [6] Development of Pressure Calibration Method in High-Pressure THz ESR System
    Sakurai, Takahiro
    Yasutani, Yoshimasa
    Sugawara, Hitoshi
    Okubo, Susumu
    Ohta, Hitoshi
    APPLIED MAGNETIC RESONANCE, 2022, 53 (3-5) : 763 - 775
  • [7] High-pressure resistance of PuTe up to 25 GPa
    Ichas, V
    Griveau, JC
    Rebizant, J
    Spirlet, JC
    PHYSICAL REVIEW B, 2001, 63 (04):
  • [8] High-pressure viscosity measurements of traction oils up to 2GPa at up to 200°C
    Nakamura, Y
    Sanda, K
    Matsubo, H
    JOURNAL OF JAPANESE SOCIETY OF TRIBOLOGISTS, 2005, 50 (04) : 354 - 359
  • [9] Development of High-Pressure ESR System Using Micro-coil
    Kohei Kawasaki
    Takahiro Sakurai
    Eiji Ohmichi
    Susumu Okubo
    Hitoshi Ohta
    Kazuyuki Matsubayashi
    Yoshiya Uwatoko
    Applied Magnetic Resonance, 2015, 46 : 987 - 992
  • [10] Development of High-Pressure ESR System Using Micro-coil
    Kawasaki, Kohei
    Sakurai, Takahiro
    Ohmichi, Eiji
    Okubo, Susumu
    Ohta, Hitoshi
    Matsubayashi, Kazuyuki
    Uwatoko, Yoshiya
    APPLIED MAGNETIC RESONANCE, 2015, 46 (09) : 987 - 992
12345