Synthesis, crystal structure and optical properties of Ba5V3O12F

被引：16
|
作者：
Kang, Jing [1 ,2 ,3 ,4 ]
Yang, Yun [1 ,2 ,3 ]
Pan, Shilie [1 ,2 ,3 ]
Yu, Hongwei [1 ,2 ,3 ,4 ]
Zhou, Zhongxiang [1 ,2 ,3 ]
机构：
[1] Key Lab Funct Mat & Devices Special Environm CAS, Xian, Peoples R China
[2] Xinjiang Key Lab Elect Informat Mat & Devices, Urumqi, Peoples R China
[3] Xinjiang Tech Inst Phys & Chem CAS, Urumqi 830011, Peoples R China
[4] Univ Chinese Acad Sci, Beijing 100049, Peoples R China
来源：
JOURNAL OF MOLECULAR STRUCTURE | 2014年 / 1056卷
基金：
中国国家自然科学基金;
关键词：
Ba5V3O12F; Apatite; Vanadium-oxide-based compounds; Synthesis; Crystal structure; LOCKED ND-LUVO4 LASER; POLAR OXIDES; LUMINESCENT PROPERTIES; APATITE-STRUCTURE; VANADIUM; GROWTH;
D O I：
10.1016/j.molstruc.2013.10.009
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
Colorless and transparent Ba(5)V(3)O(12)Fcrystal has been synthesized by solid state reaction and characterized by single-crystal X-ray diffraction and physical properties analyses. Ba5V3O12F crystallizes in the hexagonal system with space group P6(3)/m. The structure of apatite-like compound Ba5V3O12F can be described on the basis of a "framework" made of Ba(2)O-6 polyhedra and VO4 tetrahedra, which form [0 0 1]-channels filled with Ba(1) cations and F anions. The VO4 groups presented in the sample are identified by Fourier transform infrared spectrum. UV-Vis-NIR diffuse reflectance spectrum of Ba5V3O12F shows that it has a wide transmittance range from 322 to 2600 nm. Crown Copyright (C) 2013 Published by Elsevier B.V. All rights reserved.
引用
收藏
页码：79 / 83
页数：5
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