A novel fused phosphorus heterocycle:: 4-(1′, 2′, 3′, 4′-tetrahydro-1, 3, 2-benzodiazaphosphorin-2′-sulfide)-3, 4b, 4a-thiazphosphaphenanthridine derivative

被引：0

作者：

Huang, JM ^{[1
]}

Chen, H ^{[1
]}

Chen, RY ^{[1
]}

机构：

[1] Nankai Univ, Inst Elementoorgan Chem, Natl Lab Elemento Organ Chem, Tianjin 300071, Peoples R China

来源：

CHINESE CHEMICAL LETTERS | 2002年 / 13卷 / 02期

关键词：

synthesis; 3; 4b; 4a; thiazphosphaphenanthridine;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The first example of fused phosphorus heterocyclic 4-[1'-(beta-bromoethyl)-4'-oxo-3'-prop yl-1', 2', 3', 4'-tetrahydro-1, 3, 2-benzodiazaphosphorin-2'-sulfide]-1, 2, 3, 4, 4a, 4b, 5, 6-octahydro -6-oxo-5-propyl-3, 4b, 4a-thiazphosphaphenanthridine 4a, 2'-dioxide was synthesized in excellent yield by refluxing a mixture of 1-(2-bromoethyl)-2, 3-dihydro-3-propyl-1, 3, 2-benzodiazaphos phorin-4(1H)-one 2-oxide with carbon disulfide in benzene in the presence of triethylamine.

引用

页码：125 / 128

页数：4

共 50 条

[41] THE HOFMANN DEGRADATION OF 1-2-3-4-TETRAHYDRO-1-2-DI-METHYLISOQUINOLINE
CHILDS, G
FORBES, EJ
JOURNAL OF THE CHEMICAL SOCIETY, 1959, (JUN): : 2024 - 2027
[42] 2,3,4,9-Tetrahydro-1H-carbazole
Murugavel, S.
Kannan, P. S.
SubbiahPandi, A.
Surendiran, T.
Balasubramanian, S.
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O2433 - U3252
[43] 4-[4-(benzyloxy)phenyl]-1,1,1-trifluoro-4-hydroxybut-3-en-2-one
Wang, Dun-Jia
Fan, Ling
Zheng, Jing
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O2979 - U3021
[44] STUDIES IN 1,3,4,5-TETRAHYDRO-2-BENZOTHIEPINS
BOHME, H
HAACK, B
CHEMISCHE BERICHTE-RECUEIL, 1968, 101 (09): : 2971 - &
[45] 4-Phenyl-1-(2,4,5-tricyanophenyl)-1,2,3,4-tetrahydro-naphthalene
Zhang, M
Usman, A
Razak, IA
Fun, HK
Chantrapromma, S
Xu, JH
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2002, 58 : o132 - o133
[46] THE REACTION OF 3-4-DIHYDRO-4-OXOBENZO-1-2-3-TRIAZINE WITH PHOSPHORUS PENTACHLORIDE AND PHOSPHORUS OXYCHLORIDE
BUCKLEY, D
GIBSON, MS
JOURNAL OF THE CHEMICAL SOCIETY, 1956, (AUG): : 3242 - 3243
[47] 1-2-3-4-TETRAHYDRO-6-HYDROXYCARBAZOLE AND 3-HYDROXYCARBAZOLE
MILNE, AH
TOMLINSON, ML
JOURNAL OF THE CHEMICAL SOCIETY, 1952, (JUL): : 2789 - 2791
[48] EXPERIMENTS WITH 1-2-3-4-TETRAHYDRO-3-METHYLQUINAZOLINE AND RELATED COMPOUNDS
OSBORN, AR
SCHOFIELD, K
JOURNAL OF THE CHEMICAL SOCIETY, 1956, (OCT): : 3977 - 3979
[49] Synthesis of Some Novel Fused Pyrimido[4",5":5′,6′]- [1,2,4]triazino[3′,4′:3,4] [1,2,4]triazino[5,6-b]indoles with Expected Anticancer Activity
Ali, Rania S.
Saad, Hosam A.
MOLECULES, 2018, 23 (03):
[50] Stereoselective Synthesis of Novel 2-Alkenyl-2,3,4,5-tetrahydro-1,4-epoxy-1-benzazepines and 2-Alkenyl-2,3,4,5-tetrahydro-1H-1-benzazepin-4-ols
Acosta Quintero, Lina Maria
Palma, Alirio
Nogueras, Manuel
Cobo, Justo
SYNTHESIS-STUTTGART, 2012, 44 (24): : 3765 - 3782

← 1 2 3 4 5 →