A novel fused phosphorus heterocycle:: 4-(1′, 2′, 3′, 4′-tetrahydro-1, 3, 2-benzodiazaphosphorin-2′-sulfide)-3, 4b, 4a-thiazphosphaphenanthridine derivative

被引：0

作者：

Huang, JM ^{[1
]}

Chen, H ^{[1
]}

Chen, RY ^{[1
]}

机构：

[1] Nankai Univ, Inst Elementoorgan Chem, Natl Lab Elemento Organ Chem, Tianjin 300071, Peoples R China

来源：

CHINESE CHEMICAL LETTERS | 2002年 / 13卷 / 02期

关键词：

synthesis; 3; 4b; 4a; thiazphosphaphenanthridine;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The first example of fused phosphorus heterocyclic 4-[1'-(beta-bromoethyl)-4'-oxo-3'-prop yl-1', 2', 3', 4'-tetrahydro-1, 3, 2-benzodiazaphosphorin-2'-sulfide]-1, 2, 3, 4, 4a, 4b, 5, 6-octahydro -6-oxo-5-propyl-3, 4b, 4a-thiazphosphaphenanthridine 4a, 2'-dioxide was synthesized in excellent yield by refluxing a mixture of 1-(2-bromoethyl)-2, 3-dihydro-3-propyl-1, 3, 2-benzodiazaphos phorin-4(1H)-one 2-oxide with carbon disulfide in benzene in the presence of triethylamine.

引用

页码：125 / 128

页数：4

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