Synthesis of a Series of Novel Tetra-tert-butylcalix[4]arene Linked to 1,2,4-Triazole and 1,3,4-Oxadiazole Derivatives

被引:4
|
作者
Ghezelbash, Zahra Dono [1 ]
Dilmaghani, Karim Akbari [1 ]
机构
[1] Urmia Univ, Fac Chem, Dept Organ Chem, Orumiyeh 57159, Iran
关键词
Tetra-tert-butylcalix[4]arene; 1,2,4-triazole-5-thione; 1,3,4-oxadiazole-5-thione; macrocycle; ANTIMICROBIAL ACTIVITY; CALIXARENES; BEARING; ESTERS; AGENTS; 2,4-DIHYDRO-1,2,4-TRIAZOLE-3-THIONES; THIOSEMICARBAZONES; CALIX<4>ARENES; CONFORMATION; ANALOGS;
D O I
10.17344/acsi.2016.2637
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A series of tetra-tert-butylcalix[4] arene linked to 1,2,4-triazole-5-thiones and 1,3,4-oxadiazole-5-thiones derivatives at lower rim were synthesized by the reaction of 1,2,4-triazole-5-thione and 1,3,4-oxadiazole-5-thione with 5,11,17,23-tetra-tert-butyl-25,27-bis(3-bromopropoxy)-26,28-dihydroxycalix[4] arene (2). The synthesized compounds were characterized by FT-IR, H-1 NMR, C-13 NMR spectral data, elemental analysis and ESI-MS.
引用
收藏
页码:790 / 797
页数:8
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