Optimization of headspace sampling using solid-phase microextraction for volatile components in tobacco

被引：44
|
作者：
Yang, SS [1 ]
Huang, CB [1 ]
Smetena, I [1 ]
机构：
[1] Philip Morris Inc, Res Ctr, RD&D, Richmond, VA 23234 USA
来源：
JOURNAL OF CHROMATOGRAPHY A | 2002年 / 942卷 / 1-2期
关键词：
optimization; headspace sampling; tobacco; solid-phase microextraction; volatile compounds;
D O I：
10.1016/S0021-9673(01)01376-0
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
Solid-phase microextraction (SPME) was evaluated as a tool for headspace sampling of tobacco samples. Several experimental parameters (e.g. sampling temperature, pH, moisture, and the type of SPME fibers) were optimized to improve sampling efficiency in two aspects; maximum adsorption and selective adsorption of volatile components onto SPME fibers. The effect of these parameters was often dominated by the physical and chemical nature (e.g. volatility, polarity) of target compounds, thus, SPME sampling conditions can be adjusted to favor a selected group of compounds, such as organic acids in tobacco. (C) 2002 Elsevier Science B.V. All rights reserved.
引用
收藏
页码：33 / 39
页数：7
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