Comparison of headspace solid-phase microextraction with conventional extraction for the analysis of the volatile components in Melia azedarach

被引：20

作者：

Yang, Yanqin ^{[1
,3
]}

Xiao, Yanmeng ^{[1
,3
]}

Liu, Baofeng ^{[1
]}

Fang, Xuexun ^{[2
]}

Yang, Wei ^{[1
]}

Xu, Jingwei ^{[1
]}

机构：

[1] Chinese Acad Sci, Changchun Inst Appl Chem, State Key Lab Electroanalyt Chem, Changchun 130022, Jilin, Peoples R China

[2] Jilin Univ, Minist Educ, Key Lab Mol Enzymol & Enzyme Engn, Changchun 130012, Jilin, Peoples R China

[3] Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China

来源：

TALANTA | 2011年 / 86卷

关键词：

Headspace solid-phase microextraction; Ultrasonic extraction; Soxhlet extraction; GC-MS; Volatile components; Melia azedarach; ESSENTIAL OILS; LIMONOIDS; TOOSENDAN; FRUIT; IDENTIFICATION; OPTIMIZATION; SPECTROMETRY; TERPENOIDS; FIBERS;

D O I：

10.1016/j.talanta.2011.09.028

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The volatile compositions of Melia azedarach were studied by headspace solid-phase microextraction (HS-SPME). The result was compared with that obtained by soxhlet extraction (SE) and ultrasonic extraction (UAE). 79 compounds were identified in this study, among which 64 compounds were first reported. The experimental parameters including fiber type (PDMS, PDMS-DVB and CAR-PDMS), desorption time, extraction temperature and time were investigated. 37 compounds were obtained by HS-SPME, including curcumene (33.25%), alpha-cadinol (11.16%), alpha-muurolene (8.72%), copaene (5.04%), beta-bisabolene (3.41%), and a-selinene (2.97%). The result suggested that the HS-SPME method is a powerful analytic tool and complementary to traditional methods for the determination of the volatile compounds in Chinese herbs. (C) 2011 Elsevier B.V. All rights reserved.

引用

页码：356 / 361

页数：6

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