Simple and convenient synthesis of (±)-bakuchiol

被引：10
|
作者：
Chen, Hongli [1 ]
Li, Yuanchao [1 ]
机构：
[1] Chinese Acad Sci, Shanghai Inst Mat Med, Shanghai 201203, Peoples R China
来源：
LETTERS IN ORGANIC CHEMISTRY | 2008年 / 5卷 / 06期
关键词：
(+/-)-bakuchiol; citral; 1,4-addition; Grignard reagent;
D O I：
10.2174/157017808785740499
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A simple and convenient synthesis of (+/-)-bakuchiol has been developed. The key intermediate was obtained in only one step from the easily available starting material, citral, by an 1,4-addition procedure. (+/-)-Bakuchiol was finally produced in 4 steps to give 50% overall yield.
引用
收藏
页码：467 / 469
页数：3
相关论文
共 50 条
  • [1] A SIMPLE AND CONVENIENT SYNTHESIS OF PENTACHLOROZIRCONATES
    HUGHES, T
    MEREDITH, C
    SUTCLIFFE, H
    JOURNAL OF THE LESS-COMMON METALS, 1987, 134 (01): : L5 - L8
  • [2] A simple and convenient synthesis of pyrazinones
    Das Sharma, Saikat
    Gogoi, Pranjal
    Konwar, Dilip
    SYNTHETIC COMMUNICATIONS, 2007, 37 (1-3) : 107 - 111
  • [3] A Simple and Convenient Synthesis of Triprolidine
    Rao, G. Venkateswara
    Swamy, B. Narayana
    Kumar, P. Hareesh
    Reddy, G. Chandrasekara
    ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 2009, 41 (02) : 168 - 171
  • [4] A CONVENIENT SYNTHESIS OF SIMPLE TETRAHYDROISOQUINOLINES
    RUCHIRAWAT, S
    CHAISUPAKITSIN, M
    PATRANUWATANA, N
    CASHAW, JL
    DAVIS, VE
    SYNTHETIC COMMUNICATIONS, 1984, 14 (13) : 1221 - 1228
  • [5] A CONVENIENT SYNTHESIS OF A SIMPLE COUMARIN
    ISHII, H
    KANEKO, Y
    MIYAZAKI, H
    HARAYAMA, T
    CHEMICAL & PHARMACEUTICAL BULLETIN, 1991, 39 (11) : 3100 - 3102
  • [6] A convenient and simple synthesis of sorokiniol
    Kraft, Oliver
    Al-Harrasi, Ahmed
    Csuk, Rene
    PHYTOCHEMISTRY LETTERS, 2020, 39 : 8 - 11
  • [7] SYNTHESIS OF (+-)-BAKUCHIOL
    CARNDUFF, J
    MILLER, JA
    JOURNAL OF THE CHEMICAL SOCIETY C-ORGANIC, 1968, (21): : 2671 - &
  • [8] SYNTHESIS OF (+-)-BAKUCHIOL
    CARNDUFF, J
    MILLER, JA
    CHEMICAL COMMUNICATIONS, 1967, (12) : 606 - &
  • [9] A SIMPLE AND CONVENIENT METHOD FOR THE SYNTHESIS OF OLIVETOLS
    BAEK, SH
    KIM, YO
    BULLETIN OF THE KOREAN CHEMICAL SOCIETY, 1993, 14 (02) : 272 - 274
  • [10] SIMPLE AND CONVENIENT SYNTHESIS OF A PHOTODEGRADATIVE POLYIMIDE
    IIZAWA, T
    WATANABE, S
    NISHIKUBO, T
    JOURNAL OF POLYMER SCIENCE PART C-POLYMER LETTERS, 1989, 27 (11) : 411 - 415
12345