ONE STEP PROTOCOL AND GREEN SYNTHESIS OF 2-N,N-DIMETHYLAMINO-3-ALKYL(ARYL)-2-OXIDO-1-HYDRO-2-BENZO[1,3,2]DIAZAPHOSPHININE-4-ONE DERIVATIVES

被引：1

作者：

Amor, A. Ben Hadj ^{[1
]}

Abderrahim, R. ^{[1
]}

机构：

[1] Univ Carthage, Fac Sci Bizerte, LR Ressource Materiaux & Ecosyst, Mat Lamellaires & Nanomat Hybrides, Bizerte 7021, Tunisia

来源：

BULLETIN OF THE CHEMICAL SOCIETY OF ETHIOPIA | 2022年 / 36卷 / 04期

关键词：

Anthranilic acid; N; N-Dimethylphosphoramic dichloride; Diazaphosphinine; 2-OXIDES;

D O I：

10.4314/bcse.v36i4.11

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

2-N,N-dimethylamino-2-oxido-3-alkyl(aryl)-1-hydro-2-b enzo[1,3,2]diazaphosphinin-4-one (2) derivatives are synthesized by one pot reaction by reacting equimolar quantities of anthranilic acid, primary amine, and N,N-dimethylphosphoramic dichloride under reflux of ethanol with good yields. The structure of the compounds were established on the basis of their infrared, nuclear magnetic resonance spectral data (H-1 NMR, C-13 NMR and 31P NMR), mass spectrometry, and elemental analysis.

引用

页码：859 / 864

页数：6

共 50 条

[1] SYNTHESIS OF 3-(N,N-DIMETHYLAMINO)-2H-1-BENZOPYRAN-2-ONE
HRNCIAR, P
GAPLOVSKY, A
DONOVALOVA, J
TETRAHEDRON LETTERS, 1989, 30 (13) : 1709 - 1710
[2] SYNTHESIS OF 1-ARYL-3-PYRROLIN-2-ONE DERIVATIVES
TABEI, K
ITO, H
TAKADA, T
HETEROCYCLES, 1981, 16 (05) : 795 - 798
[3] Synthesis of Chalcogenides and Metal Complex of 2-Phenyl-benzo[1,3,2]dioxophosphinin-4-one
Rani, Manju
Shukla, Davender Kumar
Khan, Arif Ali
ASIAN JOURNAL OF CHEMISTRY, 2014, 26 (07) : 1998 - 2000
[4] COMPOUNDS INVOLVING THE 5,6-BENZO-1,3,2-DIAZAPHOSPHORINANE-4-ONE RING-SYSTEM - SYNTHESIS OF 2-CHLORO-SUBSTITUTED, 2-N,N-DIMETHYLAMINO-SUBSTITUTED AND 2-BIS-(2-CHLOROETHYL)AMINO-SUBSTITUTED DERIVATIVES WITH 3- AND 4-COORDINATED PHOSPHORUS
SONNENBURG, R
NEDA, I
FISCHER, A
JONES, PG
SCHMUTZLER, R
ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 1994, 49 (06): : 788 - 800
[5] Synthesis of 2-aryl-2H-[1,2,4]triazoloquinolin-3-one and 2-aryl-2H-[1,2,4]triazoloisoquinolin-3-one derivatives from α-chloroformylarylhydrazines hydrochloride
Huang, Jiann-Jyh
Chen, Kun-Lung
Lin, Yu-Shiang
Yang, Sheng-Chuan
Chuang, Shih-Hsien
Chiang, Kuo-Chen
Tseng, Wen-Che
Wong, Fung Fuh
Yeh, Mou-Yung
TETRAHEDRON, 2010, 66 (04) : 930 - 934
[6] Synthesis and antimicrobial activity of N-(substitutedphenyl)-N′-[ 1,2,3,4-tetrahydro-2-oxido-1,3,2-benzodiazaphosphorine-2-yl] ureas
Rao, LN
Reddy, CD
Reddy, BS
INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2001, 40 (09): : 817 - 821
[7] One-step synthesis of N-alkyl-2-aryl-2-oxoacetamides and N2,N4-dialkyl-2-aryl-4H-1,3-benzodioxine-2,4-dicarboxamides
Yavari, I
Djahaniani, H
TETRAHEDRON LETTERS, 2006, 47 (09) : 1477 - 1481
[8] Synthesis of copolymer of 1,3-dioxan-2-one and 2-hydro-2-oxo-1,3,2-dioxaphosphorinane
Hu, B
Zhuo, RX
Fan, CL
POLYMERS FOR ADVANCED TECHNOLOGIES, 1998, 9 (02) : 145 - 149
[9] Synthesis of 3-(1-aryl-2-mercaptoimidazolyl)-2H-1-benzopyran-2-one derivatives
Kumar, VR
Rao, VR
INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2002, 41 (02): : 415 - 418
[10] Green Synthesis of New Boron-Containing Quinazolines: Preparation of Benzo[d][1,3,2]diazaborinin-4(1H)-one Derivatives
Mahdavi, Mohammad
Asadi, Mehdi
Saeedi, Mina
Tehrani, Maryam Hosseinpour
Mirfazli, Seyedeh Sara
Shafiee, Abbas
Foroumadi, Alireza
SYNTHETIC COMMUNICATIONS, 2013, 43 (21) : 2936 - 2942

← 1 2 3 4 5 →