Inclusion complex of (S)-1,3-butanediol with (S,S)-(+)-trans-2,3-bis(hydroxydiphenylmethyl)-1,4-dioxaspiro[4.4]nonane

被引：1

作者：

Nishikawa, K

Matsumoto, A

Tsukada, H

Shiro, M

Toda, F

机构：

[1] RIGAKU CORP,XRAY RES INST,AKISHIMA,TOKYO 196,JAPAN

[2] EHIME UNIV,FAC ENGN,DEPT APPL CHEM,MATSUYAMA,EHIME 790,JAPAN

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1997年 / 53卷

关键词：

D O I：

10.1107/S0108270196014175

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

(S)-1,3-Butanediol (guest), C4H10O2, was found to be resolved from the racemate by inclusion crystallization with (S,S)-(+)-trans-2,3-bis(hydroxydiphenylmethyl)-1,4-dioxaspiro[4.4]nonane (host), C33H32O4. The unit cell of the crystal contains two pairs of host and guest molecules. There are four crystallographically independent hydrogen bonds, which form a belt-like structure along the b axis of the unit cell. The inclusion complex appears to be stabilized by hydrogen bonds and van der Waals interactions.

引用

页码：351 / 353

页数：3

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