Inclusion complex of (S)-1,3-butanediol with (S,S)-(+)-trans-2,3-bis(hydroxydiphenylmethyl)-1,4-dioxaspiro[4.4]nonane

被引：1

作者：

Nishikawa, K

Matsumoto, A

Tsukada, H

Shiro, M

Toda, F

机构：

[1] RIGAKU CORP,XRAY RES INST,AKISHIMA,TOKYO 196,JAPAN

[2] EHIME UNIV,FAC ENGN,DEPT APPL CHEM,MATSUYAMA,EHIME 790,JAPAN

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1997年 / 53卷

关键词：

D O I：

10.1107/S0108270196014175

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

(S)-1,3-Butanediol (guest), C4H10O2, was found to be resolved from the racemate by inclusion crystallization with (S,S)-(+)-trans-2,3-bis(hydroxydiphenylmethyl)-1,4-dioxaspiro[4.4]nonane (host), C33H32O4. The unit cell of the crystal contains two pairs of host and guest molecules. There are four crystallographically independent hydrogen bonds, which form a belt-like structure along the b axis of the unit cell. The inclusion complex appears to be stabilized by hydrogen bonds and van der Waals interactions.

引用

页码：351 / 353

页数：3

共 50 条

[31] Alternate poly(amide-imide)s based on 1,4-and 1,3-bis(4-trimellitimido)benzene and their mixtures
Ruei-Shin Chen
Chin-Ping Yang
Journal of Polymer Research, 1998, 5 : 233 - 241
[32] 1,3-Bis{(+)-(S)-[1-(1-naphthyl)ethyl]iminomethyl}benzene dichloromethane solvate
Espinosa Leija, Armando
Hernandez, Guadalupe
Cruz, Sandra
Bernes, Sylvain
Gutierrez, Rene
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O1316 - U2188
[33] Alternate poly(amide-imide)s based on 1,4- and 1,3-bis(4-trimellitimido)benzene and their mixtures
Chen, RS
Yang, CP
JOURNAL OF POLYMER RESEARCH-TAIWAN, 1998, 5 (04): : 233 - 241
[34] METABOLISM OF (R,S)-1,3-BUTANEDIOL ACETOACETATE ESTERS, POTENTIAL PARENTERAL AND ENTERAL NUTRIENTS IN CONSCIOUS PIGS
DESROCHERS, S
DUBREUIL, P
BRUNET, J
JETTE, M
DAVID, F
LANDAU, BR
BRUNENGRABER, H
AMERICAN JOURNAL OF PHYSIOLOGY-ENDOCRINOLOGY AND METABOLISM, 1995, 268 (04): : E660 - E667
[35] ISOLATION OF EPISULFONES FROM THE RAMBERG-BACKLUND REARRANGEMENT .2. X-RAY MOLECULAR-STRUCTURE OF 2,3-EPITHIO-8,8-DIMETHYL-6,10-DIOXASPIRO[4.5]-DECANE S,S-DIOXIDE AND OF R-6-BENZYL-T-7,T-8-EPITHIO-1,4-DIOXASPIRO[4.4]NONANE S,S-DIOXIDE
JEFFERY, SM
SUTHERLAND, AG
PYKE, SM
POWELL, AK
TAYLOR, RJK
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1993, (19): : 2317 - 2327
[36] (S,S)-1,3-BIS[(2-METHOXYETHOXY)METHOXY]-1,3-DIPHENYLACETONE - A NEW CHIRAL KETONE WITH C2 SYMMETRY
BRAUN, M
MORITZ, J
CHEMISCHE BERICHTE, 1989, 122 (06) : 1215 - 1217
[37] 1,4-DI-O-ALKYL THREITOLS FROM TARTARIC ACID - 1,4-DI-O-BENZYL-L-THREITOL - (2,3-BUTANEDIOL, 1,4-BIS(PHENYLMETHOXY) [S-(R-STAR,R-STAR)])
MASH, EA
NELSON, KA
VANDEUSEN, S
HEMPERLY, SB
ORGANIC SYNTHESES, 1990, 68 : 92 - 103
[38] (R,R)-(-)-trans-1,4-Dioxaspiro[4,5]decane-2,3-diylbis(diphenylmethanol) N-allyl-N-propyl-3-oxo-1-cyclohexenecarboxamide (2/1 inclusion compound)
Ohba, S
Miyamoto, H
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 : O646 - O648
[39] A NOVEL TYPE OF CHIRAL DIPHOSPHINE LIGAND, TRANS-2,3-BIS(DIPHENYLPHOSPHINO)-1-METHYL-1-CYCLOPROPANECARBOXYLIC ACID AND ASYMMETRIC ALLYLIC ALKYLATION BY THE USE OF ITS PALLADIUM COMPLEX
OKADA, Y
MINAMI, T
YAMAMOTO, T
ICHIKAWA, J
CHEMISTRY LETTERS, 1992, (04) : 547 - 550
[40] Synthesis and Pharmacological Properties of 1,3-Bis[(S)Phenylethyl]Imidazolidine-2-Thione
Muhammad Naveed Umar
Mohammad Shoaib
Mohammad Sadiq
Muhammad Ayaz
Sumaira Miskeen
Ismail Shah
Imran Khan
Haroon Ur Rahid
Ikram Ilahi
Sher Wali Khan
Pharmaceutical Chemistry Journal, 2016, 50 : 382 - 387

← 1 2 3 4 5 →