MEPROS - Modular electron paramagnetic resonance operating software for multifunctional high-frequency EPR spectrometer

被引:2
|
作者
Sedivy, Mattus [1 ,2 ]
Santana, Vinicius [1 ]
Sojka, Antonin [1 ]
Laguta, Oleksii [1 ]
Neugebauer, Petr [1 ]
机构
[1] Brno Univ Technol BUT, Cent European Inst Technol CEITEC, Magneto Opt & THz Spect, Brno, Czech Republic
[2] Brno Univ Technol, Fac Elect Engn & Commun, Dept Microelect, Brno, Czech Republic
基金
欧盟地平线“2020”;
关键词
Electron paramagnetic resonance; LabVIEW; Zeeman diagram; Software; Instrumentation; Automation; RAPID-SCAN EPR; LABVIEW PROGRAM; SPIN; RELAXATION; GENERATION; COMPLEXES; TRANSPORT;
D O I
10.1016/j.jmr.2023.107556
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
We present a software solution developed in LabVIEW for a home-built High-Frequency Electron Paramagnetic Resonance (HF-EPR) spectrometer. A modular approach was applied to control the spectrometer subsystems and simplify the adaptation to hardware changes during the development. The solution implements measuring procedures for conventional Continuous Wave EPR (CW-EPR), Frequency-Swept EPR (FS-EPR), and Two -Dimensional EPR (2D-EPR) mapping, which are relevant in different cases. The software's automation capa-bilities were tested in several trial measurements to obtain CW-EPR spectra of Silicon Carbide doped by vana-dium (SiC + V) at various temperatures and microwave frequencies, multi-frequency spectra via 2D-EPR mapping, and dense FS-EPR data of a lithium phthalocyanine crystal rotated in a magnetic field. Several pro-spective modifications of the software are discussed in the conclusion. A modular character allows the easy re-use of code portions in other experimental setups. The spectrometer and the software are currently deployed and utilized in a laboratory of EPR spectroscopy at Central European Institute of Technology (CEITEC) in Brno, and data obtained by it has been already used in a number of publications.
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页数:9
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